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CAS No. : | 43080-50-8 | MDL No. : | |
Formula : | C17H10O9 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | NDEURWFVDGQGAG-UHFFFAOYSA-N |
M.W : | 358.26 | Pubchem ID : | 22340255 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
44% | Stage #1: 5,5'-carbonyl-di-isophthalic acid With thionyl chloride for 6h; Reflux; Stage #2: 5-Hexen-1-ol With pyridine In dichloromethane at 20℃; for 6h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
78% | With methanol; sodium hydroxide for 8h; Reflux; | |
75% | Stage #1: tetramethyl-5,5'-carbonyldiisophthalate With sodium hydroxide In methanol for 8h; Reflux; Stage #2: With hydrogenchloride In methanol; water |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
47% | With tetrafluoroboric acid In water at 85℃; for 72h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1.1: fuming sulphuric acid / 120 °C 1.2: 1 h / Reflux 2.1: acetic anhydride; chromium(VI) oxide / 20 °C 3.1: sodium hydroxide / methanol / 8 h / Reflux |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
52% | With tetrafluoroboric acid at 90℃; Sealed tube; | 2.2. Preparation and characterization for catena-[(μ-5,5’-carbonylbis(benzene-1,3-dicarboxylato))-bis-aqua-bis-zinc(II) dimethylformamide] (1) and catena-[(μ-5,5’-carbonylbis(benzene-1,3-dicarboxylato))-bis-zinc(II)] (1a) A mixture of H4cipa of 10mg and 0.028 mmol along with Zn(NO3)2*6H2O, which was 20mg and 0.083 mmol, were mixed with HBF4 (50% in H2O, 0.6 mL) and DMF (2.0 mL).The mixture was transferred to a vial with a screw cap, which was sealed and heatedin the oven for three days at 90 °C. Colorless single crystals with block-shape were collectedand then washed using DMF several times to obtain 1 and the yield was 8mg(52% on the basis of ligand H4cipa). Anal. Calcd for 1 (C20H17NO12Zn2): C, 40.43; H,2.88; N, 2.36%. Found for 1: C, 40.23; H, 2.77; N, 2.54%. Main FT-IR absorptions (KBrpellets, cm-1): 3382, 2973, 1646, 1447, 1378, 1286, 1044, 734. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
90% | With sodium tetrahydridoborate; sodium hydroxide In methanol; lithium hydroxide monohydrate at 20℃; for 4.5h; |