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[ CAS No. 4363-34-2 ] {[proInfo.proName]}

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Chemical Structure| 4363-34-2
Chemical Structure| 4363-34-2
Structure of 4363-34-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 4363-34-2 ]

CAS No. :4363-34-2 MDL No. :MFCD02258951
Formula : C2H5BO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :71.87 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 4363-34-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 4363-34-2 ]
  • Downstream synthetic route of [ 4363-34-2 ]

[ 4363-34-2 ] Synthesis Path-Upstream   1~4

  • 1
  • [ 123-91-1 ]
  • [ 2005-43-8 ]
  • [ 4363-34-2 ]
  • [ 772-03-2 ]
YieldReaction ConditionsOperation in experiment
60% With potassium carbonate In water 18.2
2-Vinylquinoline
A mixture of 2-bromoquinoline (5.00 g, 24.03 mmol), vinylboronic acid (2.07 g, 28.83 mmol), K2CO3 (9.96 g, 72.08 mmol) and Pd(dppf)Cl2 (1.96 g, 2.403 mmol) in water (10 mL) and 1,4-dioxane (30 mL) was stirred at 105° C. overnight.
The mixture was diluted with EtOAc (100 mL) and washed with brine (30 mL*4).
The organic layer was dried over Na2SO4, filtered and concentrated in vacuo.
The residue was purified on a silica column (PE/EtOAc=20:1, v/v) to afford the title product as a light orange oil (2.25 g, yield 60percent). LCMS (ESI+): m/z 156 (M+H)+, Rt: 1.89 min.
Reference: [1] Patent: US2013/5705, 2013, A1,
  • 2
  • [ 4363-34-2 ]
  • [ 6630-33-7 ]
  • [ 28272-96-0 ]
Reference: [1] European Journal of Organic Chemistry, 2004, # 5, p. 1075 - 1082
  • 3
  • [ 76-09-5 ]
  • [ 4363-34-2 ]
  • [ 75927-49-0 ]
Reference: [1] Journal of Organic Chemistry, 2003, vol. 68, # 15, p. 6031 - 6034
  • 4
  • [ 4363-34-2 ]
  • [ 4408-64-4 ]
  • [ 1104636-73-8 ]
Reference: [1] Organic Letters, 2018, vol. 20, # 17, p. 5300 - 5303
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