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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 44398-42-7 Chemical Structure| 44398-42-7

Structure of 44398-42-7

Chemical Structure| 44398-42-7

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Product Details of [ 44398-42-7 ]

CAS No. :44398-42-7
Formula : C3H6ClNO
M.W : 107.54
SMILES Code : CC(NCCl)=O
MDL No. :MFCD19217835

Safety of [ 44398-42-7 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H311-H331-H341
Precautionary Statements:P201-P202-P261-P264-P270-P271-P280-P302+P352-P304+P340-P308+P313-P310-P330-P361-P403+P233-P405-P501
Class:6.1
UN#:2810
Packing Group:

Application In Synthesis of [ 44398-42-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 44398-42-7 ]

[ 44398-42-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 625-51-4 ]
  • [ 44398-42-7 ]
YieldReaction ConditionsOperation in experiment
With phosphorus pentachloride; trichlorophosphate; for 2.5h;Reflux; A compound of formula (G) (3.0 mmol) was dissolved in 10 mL of POCl3,Heat to reflux and carefully add PCl5 (6.0 mmol) in portions.The reaction was refluxed for 2.5 h, and the reaction was completed by TLC.The temperature was lowered to room temperature, and the reaction solution was poured into 200 mL of ice water. The pH of the 1NNaOH solution was adjusted to neutrality, extracted with CH2Cl2, and dried over anhydrous sodium sulfate.Filtration, concentration and purification by column chromatography provided the compound of formula (F).
 

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