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Chemical Structure| 444666-41-5 Chemical Structure| 444666-41-5

Structure of 444666-41-5

Chemical Structure| 444666-41-5

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Product Details of [ 444666-41-5 ]

CAS No. :444666-41-5
Formula : C10H15N3O
M.W : 193.25
SMILES Code : COC1=CC(N2CCNCC2)=NC=C1
MDL No. :MFCD06738951

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Application In Synthesis of [ 444666-41-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 444666-41-5 ]

[ 444666-41-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 5451-55-8 ]
  • [ 444666-41-5 ]
  • C21H33N3O2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20℃; (10 mmol) of compound II, 1.93 g (10 mmol) of compound III-1 and 20 mL of dry THF were added to a 100 mL round bottom flask and the resulting mixture was stirred under ice-cooling in an ice bath. After adding 2.48 g (12 mmol) of DCC, Stirring was continued at room temperature overnight. TLC shows the completion of the reaction. The reaction mixture was poured into ice water, stirred, extracted with 50 mL of x3 dichloromethane, and the combined organic phases were combined, washed with saturated brine, dried over anhydrous sodium sulfate, and the solvent was evaporated on a rotary evaporator. The resulting residue column Chromatography to give the product I-1 as a pale yellow solid, ESI-MS, m / z = 361 ([M + H] +). Using the method of Example 1, the following compounds having the general formula I were synthesized.
 

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