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Chemical Structure| 47168-52-5 Chemical Structure| 47168-52-5

Structure of 47168-52-5

Chemical Structure| 47168-52-5

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Product Details of [ 47168-52-5 ]

CAS No. :47168-52-5
Formula : C15H12O6
M.W : 288.25
SMILES Code : O=C(O)C1=CC=C(OCOC2=CC=C(C=C2)C(O)=O)C=C1

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Application In Synthesis of [ 47168-52-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 47168-52-5 ]

[ 47168-52-5 ] Synthesis Path-Downstream   1~1

  • 1
  • cobalt(II) sulfate [ No CAS ]
  • [ 143131-66-2 ]
  • [ 47168-52-5 ]
  • [Co(L)(1,4-bis((1H-imidazol-1-yl)methyl)benzene)0.5] [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; In methanol; N,N-dimethyl acetamide; at 100℃; for 72h;Autoclave; High pressure; To a solution of H2L (0.0576 g, 0.2 mmol) and btmb (0.024 g, 0.15 mmol) in DMA (9 mL) a solution of CoSO4 (0.0844 g, 0.3 mmol) in methanol (6 mL) was added. Further, 5 drops of 1 mol L-1 NaOH solution was added and the solution was placed in a 23 mL Parr Teflon-lined stainless steel vessel and then thevessel was sealed and heated at 100 C for 3 days. After slowly cooling to room temperature, purple crystals of 3 were obtained with an approximate yield of 53%. Anal. Calcd (%): C: 48.38, H: 0.18, N:2.56. Found (%): C: 45.04, H: 0.11, N: 2.45. FT-IR (KBr, cm-1): 1607(s), 1566(w), 1516(w), 1477(w), 1404(s),1304(w), 1279(w), 1243(w), 1207(s), 1172(s), 1152(m), 1130(w), 1098(w), 1044(w), 994(s), 855(m), 781(s),725(w), 676(w), 619(w), 455(w).
 

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