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CAS No. : | 482628-23-9 | MDL No. : | MFCD28793139 |
Formula : | C8H10BFO4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | YXCHYZQCQRCTOC-UHFFFAOYSA-N |
M.W : | 199.97 | Pubchem ID : | 22485600 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In hexane; | EXAMPLE 22 N,N'-Bis[2-(4-fluoro-3,5-dimethoxyphenyl)-5-pyridyl]-N,N'-dimethyletylenediamine dimethanesulfonate Following the procedure of Example 1, an oil was obtained from N,N'-bis(2-trifluoromethanesulfonyloxy-5-pyridyl)-N,N'-dimethylethylenediamine (150.0 mg, 0.280 5 mmol) synthesised as described in Reference Example 1 and <strong>[482628-23-9]4-fluoro-3,5-dimethoxyphenylboronic acid</strong> (167.0 mg, 0.840 mmol). Hexane was added to the oil and the resulting precipitate was collected by filtration to provide N,N'-bis[2-(4-fluoro-3,5-dimethoxyphenyl)-5-pyridyl]-N,N'-dimethylethylenediamine as a yellow crystalline powder (160.0 mg; quantitative). |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
EXAMPLE 38 1,4-Bis[5-(4-fluoro-3,5-dimethoxyphenyl)-2-pyridyl]hexahydro-1,4-diazepine Following the procedure of Example 1, the title compound was obtained as a pale yellow amorphous powder (138.9 mg, yield: 93%) from 1,4-bis(5-bromo-2-pyridyl)hexahydro-1,4-diazepine (110.0 mg, 0.270 mmol) synthesised in Reference Example 1 and <strong>[482628-23-9]4-fluoro-3,5-dimethoxyphenylboronic acid</strong> (160.0 mg, 0.800 mmol) synthesised from 1-bromo-4-fluoro-3,5-dimethoxybenzene (JP 10-87543A) synthesised by a similar procedure to that described in Reference Example 2. 1H-NMR (CDCl3) delta: 2.16 (tt, J=6.0, 6.03 Hz, 2 H), 3.64 (dd, J 6.0, 6.0 Hz, 4 H), 3.93 (s, 12 H), 3.95 (s, 4 H), 6.62 (d, J=9.0 Hz, 2 H), 6.71 (d, 4JHF=6.0 Hz, 4 H), 7.63 (dd, J=3.0, 9.0 Hz, 2 H), 8.36 (d, J=3.0 Hz, 2 H). |