Home Cart 0 Sign in  

[ CAS No. 4920-84-7 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 4920-84-7
Chemical Structure| 4920-84-7
Structure of 4920-84-7 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 4920-84-7 ]

Related Doc. of [ 4920-84-7 ]

Alternatived Products of [ 4920-84-7 ]

Product Details of [ 4920-84-7 ]

CAS No. :4920-84-7 MDL No. :MFCD00024210
Formula : C8H9NO4 Boiling Point : -
Linear Structure Formula :- InChI Key :XXWIYOBCHKCWNT-UHFFFAOYSA-N
M.W : 183.16 Pubchem ID :78633
Synonyms :

Safety of [ 4920-84-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H332-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 4920-84-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 4920-84-7 ]
  • Downstream synthetic route of [ 4920-84-7 ]

[ 4920-84-7 ] Synthesis Path-Upstream   1~5

  • 1
  • [ 446-35-5 ]
  • [ 865-33-8 ]
  • [ 446-38-8 ]
  • [ 448-19-1 ]
  • [ 4920-84-7 ]
Reference: [1] Tetrahedron Letters, 2009, vol. 50, # 27, p. 3776 - 3779
  • 2
  • [ 446-35-5 ]
  • [ 865-33-8 ]
  • [ 446-38-8 ]
  • [ 448-19-1 ]
  • [ 4920-84-7 ]
Reference: [1] Tetrahedron Letters, 2009, vol. 50, # 27, p. 3776 - 3779
  • 3
  • [ 446-35-5 ]
  • [ 124-41-4 ]
  • [ 448-19-1 ]
  • [ 4920-84-7 ]
Reference: [1] Recueil des Travaux Chimiques des Pays-Bas, 1916, vol. 35, p. 142[2] Chem. Zentralbl., 1913, vol. 84, # II, p. 760
  • 4
  • [ 4920-84-7 ]
  • [ 704-14-3 ]
YieldReaction ConditionsOperation in experiment
89% With aluminum (III) chloride In dichloromethane for 5.5 h; Reflux A solution of 2,4-dimethoxynitrobenzene (2.0 g, 10.9 mmol) in 360 mL of CH2Cl2 was cooled to 0 °C and 2.91 g of AlCl3 (21.3 mmol) were portionwise added. The mixture was heated to reflux for 5.5 h (development of a bright red color). After cooling to RT, 10percent aqueous HCl was added dropwise and the mixture was extracted three times with CH2Cl2. The combined organic layers were dried with MgSO4. After solvent removal under reduced pressure the crude product was purified bychromatography (c-hex/EtOAc = 10:1) to afford 5-methoxy-2-nitrophenol (11) as ayellow solid (1.64 g, 9.69 mmol, 89percent).
Reference: [1] Synthetic Communications, 2009, vol. 39, # 11, p. 2053 - 2057
[2] Synlett, 2015, vol. 26, # 10, p. 1395 - 1397
  • 5
  • [ 6627-53-8 ]
  • [ 124-41-4 ]
  • [ 704-14-3 ]
  • [ 4920-84-7 ]
Reference: [1] Recueil des Travaux Chimiques des Pays-Bas, 1902, vol. 21, p. 325
Same Skeleton Products
Historical Records

Related Functional Groups of
[ 4920-84-7 ]

Aryls

Chemical Structure| 6665-97-0

[ 6665-97-0 ]

1,3-Dimethoxy-2-nitrobenzene

Similarity: 1.00

Chemical Structure| 14227-18-0

[ 14227-18-0 ]

2,4,6-Trimethoxynitrobenzene

Similarity: 1.00

Chemical Structure| 16292-95-8

[ 16292-95-8 ]

3-Methoxy-4-nitrophenol

Similarity: 1.00

Chemical Structure| 3114-61-2

[ 3114-61-2 ]

3-Methoxy-2-nitrophenol

Similarity: 1.00

Chemical Structure| 704-14-3

[ 704-14-3 ]

5-Methoxy-2-nitrophenol

Similarity: 0.98

Ethers

Chemical Structure| 6665-97-0

[ 6665-97-0 ]

1,3-Dimethoxy-2-nitrobenzene

Similarity: 1.00

Chemical Structure| 14227-18-0

[ 14227-18-0 ]

2,4,6-Trimethoxynitrobenzene

Similarity: 1.00

Chemical Structure| 16292-95-8

[ 16292-95-8 ]

3-Methoxy-4-nitrophenol

Similarity: 1.00

Chemical Structure| 3114-61-2

[ 3114-61-2 ]

3-Methoxy-2-nitrophenol

Similarity: 1.00

Chemical Structure| 704-14-3

[ 704-14-3 ]

5-Methoxy-2-nitrophenol

Similarity: 0.98

Nitroes

Chemical Structure| 6665-97-0

[ 6665-97-0 ]

1,3-Dimethoxy-2-nitrobenzene

Similarity: 1.00

Chemical Structure| 14227-18-0

[ 14227-18-0 ]

2,4,6-Trimethoxynitrobenzene

Similarity: 1.00

Chemical Structure| 16292-95-8

[ 16292-95-8 ]

3-Methoxy-4-nitrophenol

Similarity: 1.00

Chemical Structure| 3114-61-2

[ 3114-61-2 ]

3-Methoxy-2-nitrophenol

Similarity: 1.00

Chemical Structure| 704-14-3

[ 704-14-3 ]

5-Methoxy-2-nitrophenol

Similarity: 0.98