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CAS No. : | 4922-51-4 | MDL No. : | MFCD07643239 |
Formula : | C8H8N4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | KTEQHOVTBRZQPC-UHFFFAOYSA-N |
M.W : | 160.18 | Pubchem ID : | 3052732 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280 | UN#: | N/A |
Hazard Statements: | H302-H317 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
EXAMPLE 6 Preparation of (3Z)-3-[4-(1H-1,2,4-triazol-3-yl)anilino]methylene}-1,3-dihydro-2H-indol-2-one Prepared in an analogous manner to Example 1 using one equivalent of <strong>[4922-51-4]4-(1H-1,2,4-triazol-3-yl)aniline</strong> in place of 5-aminobenzimidazolone. 1H NMR (400 MHz, d6-DMSO) delta14.32 (s, 1H, exchangeable); 14.05 (s, 1H, exchangeable); 10.82 (m, 1H); 10.54 (m, 1H); 8.64 (m, 1H); 8.60 (s, 1H, exchangeable); 8.00 (m, 2H); 7.63 (m, 1H); 7.47 (m, 1H); 7.03 (m, 1H); 6.94 (m, 1H); 6.85 (m, 1H). APCI MS (-ve) 302. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
By utilizing the suitable S-methyl-thioimidoylphosphonic acid monoethyl ester and substituting the following phenylamines: ... (c) 4-(3-chloro-4-amino-phenyl)-1-H-imidazole, (d) 4-(3-amino-phenyl)-1-H-imidazole, (e) 2-(4-amino-phenyl)-1-H-imidazole, (f) 3-(4-amino-phenyl)-pyrazole, or (g) 3-(4-amino-phenyl)-1,2,4-triazole |
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