Home Cart Sign in  
Chemical Structure| 51079-51-7 Chemical Structure| 51079-51-7

Structure of 51079-51-7

Chemical Structure| 51079-51-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 51079-51-7 ]

CAS No. :51079-51-7
Formula : C17H26O2
M.W : 262.39
SMILES Code : CC(C)CC(C)CC(OC1=CC=C2CCOC2=C1)C

Safety of [ 51079-51-7 ]

Application In Synthesis of [ 51079-51-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 51079-51-7 ]

[ 51079-51-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 680-31-9 ]
  • [ 23681-89-2 ]
  • [ 51079-50-6 ]
  • [ 51079-51-7 ]
YieldReaction ConditionsOperation in experiment
In tetrahydrofuran; diethyl ether; EXAMPLE 5 0.87 g. of a 55percent by weight sodium hydride dispersion in oil are washed under nitrogen three times with absolute tetrahydrofuran and subsequently covered with 8 ml. of absolute tetrahydrofuran. Thereafter, the mixture is cooled to 0° C. and treated dropwise while stirring with a solution of 2.72 g. of <strong>[23681-89-2]6-hydroxy-2,3-dihydrobenzofuran</strong> in 12 ml. of absolute tetrahydrofuran. The mixture is stirred for 1.5 hours at room temperature and again cooled to 0° C. before a solution of 4.0 g. of 1,3,5-trimethylhexyl p-toluenesulfonate in 10 ml. of absolute tetrahydrofuran is added. Subsequently, the mixture is diluted with 10 ml. of absolute hexamethylphosphoric acid triamide and stirred for 24 hours at room temperature. The mixture is poured onto ice-water and extracted three times with diethyl ether. The extracts are washed with water and saturated aqueous sodium chloride solution, dried over sodium sulfate and evaporated. By chromatography on silica gel with hexane/diethyl ether (98:2 parts by volume) there is obtained pure 6-[(1,3,5-trimethylhexyl)-oxy]-2,3 -dihydrobenzofuran which is distilled in a bulb-tube at 118° C./0.3 mmHg; nD22 = 1.5057.
 

Historical Records

Technical Information

Categories