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[ CAS No. 52536-39-7 ] {[proInfo.proName]}

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Chemical Structure| 52536-39-7
Chemical Structure| 52536-39-7
Structure of 52536-39-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 52536-39-7 ]

CAS No. :52536-39-7 MDL No. :MFCD09030814
Formula : C9H9NO Boiling Point : -
Linear Structure Formula :- InChI Key :DRGLRUYXGNMDDM-UHFFFAOYSA-N
M.W : 147.17 Pubchem ID :10773120
Synonyms :

Safety of [ 52536-39-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H302-H312-H315-H319-H332-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 52536-39-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 52536-39-7 ]

[ 52536-39-7 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 6165-75-9 ]
  • acetic acid-<2-hydroxy-phenyl>-anilide [ No CAS ]
  • [ 52536-39-7 ]
  • 3
  • [ 5326-38-5 ]
  • [ 52536-39-7 ]
  • [ 1350705-01-9 ]
  • 4
  • [ 4755-50-4 ]
  • [ 52536-39-7 ]
  • [ 1610805-28-1 ]
YieldReaction ConditionsOperation in experiment
With triethylamine In dichloromethane at 0 - 20℃; for 24h;
With triethylamine In dichloromethane at 0 - 20℃; for 26h; 5.4 General procedure for the preparation of 1c-19c General procedure: The freshly formed aromatic acyl chloride (5mmol) dissolved in dry dichloromethane (25ml) was added dropwise to a solution of compound b (5mmol) and triethylamine (6mmol) dissolved in dichloromethane (25mL), keeping the temperature at 0°C for 2h, and then, the mixture was stirred at room temperature for 24h. The reaction solution was washed by 1N hydrochloric acid (3×30mL), saturated aqueous Na2CO3 (3×30mL), and brine (2×30mL) in sequence. The organic layer was dried by anhydrous Na2SO4, then, filtered and evaporated to afford the desired product compound 1c-19c.
  • 5
  • [ 186663-74-1 ]
  • [ 52536-39-7 ]
  • 6
  • [ 23806-24-8 ]
  • [ 52536-39-7 ]
  • C15H13NO2S [ No CAS ]
  • 7
  • [ 52536-39-7 ]
  • [ 67713-99-9 ]
YieldReaction ConditionsOperation in experiment
77% General procedure: 2-Alkylpropoxyaniline compound (0.5 mmol) was sequentially added to a dry reaction tube under an argon-protected ice bath.Acetone (3.0 mL), concentrated hydrochloric acid (0.12 mL), and stirred for 5 min, then tert-butyl nitrite (0.08 mL) was added to the system.After the reaction system was stirred for 15 min in an ice bath, sodium iodide (0.2 mmol) was added, and acetone (7.0 mL) was added thereto, the ice bath was removed, and the system was heated to 60 C, and the reaction was terminated for about 9 hours.Stop stirring, remove solvent under reduced pressure, column chromatography, eluent:Ethyl acetate and petroleum ether were collected and the corresponding product A was obtained.
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