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Chemical Structure| 527681-60-3 Chemical Structure| 527681-60-3

Structure of 527681-60-3

Chemical Structure| 527681-60-3

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Product Details of [ 527681-60-3 ]

CAS No. :527681-60-3
Formula : C9H11NO2
M.W : 165.19
SMILES Code : OCC1=CC(CCCO2)=C2C=N1
MDL No. :MFCD18802895

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Application In Synthesis of [ 527681-60-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 527681-60-3 ]

[ 527681-60-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 527681-60-3 ]
  • [ 527681-61-4 ]
YieldReaction ConditionsOperation in experiment
With manganese(IV) oxide; In chloroform; for 4.83333h;Heating / reflux; To a solution of 0.25 g of (3,4-dihydro-2H-pyrano(2,3-c)pyridin-6-yl)methanol in 7.5 mL of chloroform, 0.66 g of manganese dioxide was added, and the mixture was heated under reflux while stirring for 4 hours 50 minutes. The reaction mixture was cooled to room temperature, the insoluble substance was then filtered off, and the solvent was distilled off under reduced pressure to obtain 0.24 g of 3,4-dihydro-2H-pyrano(2,3-c)pyridine-6-carbaldehyde as a light yellow oily substance. 1H-NMR (CDCl3) delta: 2.04-2.11 (2H, m), 2.85 (2H, t, J = 6.5 Hz), 4.32 (2H, t, J = 5.1 Hz), 7.72 (1H, s), 8.27 (1H, s), 9.94 (1H, s)
 

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