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Chemical Structure| 538-60-3 Chemical Structure| 538-60-3

Structure of 538-60-3

Chemical Structure| 538-60-3

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Product Details of [ 538-60-3 ]

CAS No. :538-60-3
Formula : C14H15O3P
M.W : 262.24
SMILES Code : OP(OCC1=CC=CC=C1)OCC2=CC=CC=C2

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Application In Synthesis of [ 538-60-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 538-60-3 ]

[ 538-60-3 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 538-60-3 ]
  • [ 57497-39-9 ]
  • [ 140173-68-8 ]
YieldReaction ConditionsOperation in experiment
64% With sodium hydrogencarbonate; paraformaldehyde; In tetrahydrofuran; EXAMPLE 2 Dibenzyl P-(N-tert-Butyl-N-hydroxyaminomethyl)phosphonate Using the procedure of Example 1, the above-named compound is prepared from 5.0 g (40 mmol) of <strong>[57497-39-9]N-tert-butylhydroxylamine hydrochloride</strong>, 2.4 g (80 mmol) of paraformaldehyde, 9.0 g (41 mmol) of dibenzyl phosphite, 3.0 g (40 mmol) of sodium bicarbonate and 200 ml of tetrahydrofuran (THF) by heating at 55° C. for 14 hours. The residue is purified by recrystallization from a mixture of methylene chloride and hexane to give 9.2 g (64percent yield) of a white solid melting at 106°-107° C. Analysis: Calcd for C19 H26 NO4 P: C, 62.8; H, 7.2; N, 3.8; P, 8.5. Found: C, 62.6; H, 7.1; N, 3.8; P, 8.9.
  • 2
  • [ 538-60-3 ]
  • [ 1623-07-0 ]
 

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