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[ CAS No. 53867-95-1 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 53867-95-1
Chemical Structure| 53867-95-1
Structure of 53867-95-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 53867-95-1 ]

CAS No. :53867-95-1 MDL No. :MFCD09261104
Formula : C9H8N2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 160.17 Pubchem ID :-
Synonyms :

Safety of [ 53867-95-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 53867-95-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 53867-95-1 ]

[ 53867-95-1 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 23432-46-4 ]
  • [ 53867-95-1 ]
YieldReaction ConditionsOperation in experiment
With palladium on activated charcoal; ethanol Hydrogenation;
YieldReaction ConditionsOperation in experiment
IIf, konz. HCl (Ausb.:41.4percent);
4-Ethoxy-8-aminochinolin, HI;
  • 3
  • [ 53867-95-1 ]
  • [ 4659-45-4 ]
  • 8-amino-4-(2,6-dichlorobenzoyloxy)quinoline [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine In ethanol; ISOPROPYLAMIDE; water 4.1 Example 4 (1) A mixture of 8-amino-4-hydroxyquinoline (300 mg), 2,6-dichlorobenzoyl chloride (432 mg), triethylamine (569 mg) and catalytic amount of dimethylaminopyridine in dimethylacetamide (3 ml) was stirred for 1 hour under ice-cooling. To the mixture was added water (3 ml) and the resulting precipitate was collected by filtration. The residue was suspended in hot ethanol (10 ml) with stirring. The resulting precipitate was collected by filtration, and the residue was purified by flash chromatography (ethyl acetate-dichloromethane) to give 8-amino-4-(2,6-dichlorobenzoyloxy)quinoline (240 mg). NMR (CDCl3, δ): 5.03 (2H, br s), 6.95 (1H, d, J=7.5 Hz), 7.30-7.52 (6H, m), 8.79 (1H, d, J=5 Hz)
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