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CAS No. : | 5391-74-2 | MDL No. : | MFCD00026242 |
Formula : | C9H10N2O | Boiling Point : | - |
Linear Structure Formula : | C6H5NHNCHC(O)CH3 | InChI Key : | - |
M.W : | 162.19 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
85% | With pyridine In ethanol for 1.5h; Reflux; | 6-Acetyl-3-amino-2-phenyl-5-(p-tolyl)-2,5-dihydropyridazine-4-carbonitrile (3f) General procedure: Pyridine (0.5 mL) was added to a mixture of 1-(2-phenylhydrazono)propan-2-one 1 (10 mmol, 1.62 g) and the appropriatebenzylidenemalononitrile derivative 2a-g (10 mmol) in ethanol(20 mL). The mixture was refluxed for 1.5 h and monitored by TLCusing n-hexane : ethyl acetate (2 : 1). After the completion of thereaction, the solvent was evaporated under reduced pressure andthe resulting crude product was washed with water (2 × 20 mL) andrecrystallised from ethanol |