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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 54093-33-3 Chemical Structure| 54093-33-3

Structure of 54093-33-3

Chemical Structure| 54093-33-3

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Product Details of [ 54093-33-3 ]

CAS No. :54093-33-3
Formula : C6H15NO2
M.W : 133.19
SMILES Code : OCCCNCCOC
MDL No. :MFCD12179043

Safety of [ 54093-33-3 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:2735
Packing Group:

Application In Synthesis of [ 54093-33-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 54093-33-3 ]

[ 54093-33-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 16427-44-4 ]
  • [ 156-87-6 ]
  • [ 54093-33-3 ]
YieldReaction ConditionsOperation in experiment
47% In tetrahydrofuran; for 8h;Reflux; 1.54 g of ethylene glycol monomethyl ether protected with Ms 24-2 (0.01 mol) and 7.5 g of amino-n-propanol 24-3 (0.1 mol) was dissolved in 30 mL of anhydrous tetrahydrofuran, and the mixture was reacted under refluxing for 8 hours. The reaction solution was washed with water and concentrated to obtain the crude target product 24-4. The crude product was dissolved in dichloromethane (30 mL), an appropriate amount of silica gel was added and the sample was stirred, spin-dried under reduced pressure and directly placed on a silica gel column for column chromatographic purification, with an eluent solution (dichloromethane:methanol=20/1-5/1) to obtain 0.63 g of the target product 24-4 as a pale yellow liquid, yield 47%. LC-MS: m/z=134[M+H]+.
 

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