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[ CAS No. 54579-63-4 ] {[proInfo.proName]}

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Chemical Structure| 54579-63-4
Chemical Structure| 54579-63-4
Structure of 54579-63-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 54579-63-4 ]

CAS No. :54579-63-4 MDL No. :MFCD09035494
Formula : C13H11NO3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 229.23 Pubchem ID :-
Synonyms :

Safety of [ 54579-63-4 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 54579-63-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 54579-63-4 ]

[ 54579-63-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 27237-21-4 ]
  • [ 54579-63-4 ]
YieldReaction ConditionsOperation in experiment
48% In methanol A11. Synthesis of 4-(3-Carboxyphenoxy)aniline A slurry of 4-(3-carboxyphenoxy)-1-nitrobenzene (5.38 g, 20.7 mmol) and 10% Pd/C (0.50 g) in MeOH (120 mL) was stirred under an H2 atmosphere (balloon) for 2 d. The resulting mixture was filtered through a pad of Celite, then concentrated under reduced pressure to afford 4-(3-carboxyphenoxy)aniline as a brown solid (2.26 g, 48%): TLC (10% MeOH/90% CH2Cl2) Rf 0.44 (streaking).
48% In methanol Synthesis of 4-(3-Carboxyphenoxy)aniline Synthesis of 4-(3-Carboxyphenoxy)aniline A slurry of 4-(3-carboxyphenoxy)-1-nitrobenzene (5.38 g, 20.7 mmol) and 10% Pd/C (0.50 g) in MeOH (120 mL) was stirred under an H2 atmosphere (balloon) for 2 d. The resulting mixture was filtered through a pad of Celite, then concentrated under reduced pressure to afford 4-(3-carboxyphenoxy)aniline as a brown solid (2.26 g, 48%): TLC (10% MeOH/90% CH2Cl2) Rf 0.44 (streaking).
48% In methanol 11 Step 1. A slurry of 4-(3-carboxyphenoxy)-1-nitrobenzene (5.38 g, 20.7 mmol) and 10% Pd/C (0.50 g) in MeOH (120 mL) was stirred under an H2 atmosphere (balloon) for 2 d. The resulting mixture was filtered through a pad of Celite, then concentrated under reduced pressure to afford 4-(3-carboxyphenoxy)aniline as a brown solid (2.26 g, 48%): TLC (10% MeOH/90% CH2Cl2) Rf 0.44 (streaking).
48% With hydrogen In methanol for 48h; A.A11 Synthesis of 4-(3-Carboxyphenoxy)aniline. Synthesis of 4-(3-Carboxyphenoxy)aniline. A slurry of 4-(3-carboxyphenoxy)-1-nitrobenzene (5.38 g, 20.7 mmol) and 10% Pd/C (0.50 g) in MeOH (120 mL) was stirred under an H2 atmosphere (balloon) for 2 d. The resulting mixture was filtered through a pad of Celite, then concentrated under reduced pressure to afford 4-(3-carboxyphenoxy)aniline as a brown solid (2.26 g, 48%): TLC (10% MeOH/90% CH2Cl2) Rf 0.44 (streaking).

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