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Chemical Structure| 54730-30-2 Chemical Structure| 54730-30-2

Structure of 54730-30-2

Chemical Structure| 54730-30-2

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Product Details of [ 54730-30-2 ]

CAS No. :54730-30-2
Formula : C12H14O2
M.W : 190.24
SMILES Code : O=CC1=CC=C(O)C(CC=C(C)C)=C1
MDL No. :MFCD13192050

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Application In Synthesis of [ 54730-30-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 54730-30-2 ]

[ 54730-30-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 123-08-0 ]
  • [ 870-63-3 ]
  • [ 28090-12-2 ]
  • [ 54730-30-2 ]
YieldReaction ConditionsOperation in experiment
27%; 20% at 25℃; for 24h;Alkaline conditions; Specific operation: Add p-hydroxybenzaldehyde (0.1mol), KOH (0.15mol), 120mL of pure water in a round bottom flask, slowly add bromoisopentene (0.12mol) dropwise at room temperature, continue to stir the reaction, and TLC monitor the reaction Process (petroleum ether: ethyl acetate = 5:1). After the reaction is over, adjust the pH to 3 with 3N hydrochloric acid, extract 3×100 mL with ethyl acetate, combine the organic phases, wash with saturated sodium carbonate solution, saturated brine, dry with anhydrous sodium sulfate, and evaporate the solvent under reduced pressure. The yellow oil was subjected to silica gel column chromatography (petroleum ether: ethyl acetate = 8:1) to obtain slightly yellow oils (a1) and (a2), the yield of a1: 17-20%; the yield of a2: 23-27% .
 

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