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Chemical Structure| 55129-05-0 Chemical Structure| 55129-05-0

Structure of 55129-05-0

Chemical Structure| 55129-05-0

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Product Details of [ 55129-05-0 ]

CAS No. :55129-05-0
Formula : C6H11NO
M.W : 113.16
SMILES Code : [H][C@@]12[C@@](COC2)([H])CNC1
MDL No. :MFCD16556190
InChI Key :HQQVXVKQOPZRBJ-OLQVQODUSA-N
Pubchem ID :55299467

Safety of [ 55129-05-0 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H314-H226
Precautionary Statements:P501-P270-P240-P210-P233-P243-P241-P242-P264-P280-P370+P378-P303+P361+P353-P301+P330+P331-P363-P301+P312+P330-P304+P340+P310-P305+P351+P338+P310-P403+P235-P405
Class:8(3)
UN#:2920
Packing Group:

Application In Synthesis of [ 55129-05-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 55129-05-0 ]

[ 55129-05-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 456-24-6 ]
  • [ 55129-05-0 ]
  • C11H13N3O3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
76.3% With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 110℃; for 2h; To a stirred solution of 73.1 (0.19 g, 1.336 mmol, 1.0 eq) and (3 aR,6aS)-hexahydro-1H-furo[3,4-c]pyrrole (0.2 g, 1.34 mmol, 1.0 eq) in dry DMSO (5.0 mL), was added DIPEA (2.37 mL, 13.36 mmol, 10.0 eq). The reaction was stirred at 110 C. for 2 hours. After completion of the reaction, mixture was poured into water and extracted with EtOAc. Organic layers were combined, washed with brine, dried over Na2SO4 and concentrated under reduced pressure to obtain crude material. The crude was purified by trituration to afford 73.2 (0.24 g, 76.3%). MS(ES): m/z 235.24 [M+H]+.
 

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[ 55129-05-0 ]

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