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Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
Accessible (Haz class 3, 4, 5 or 8), International USD 200+
Chemical Structure| 5565-85-5 Chemical Structure| 5565-85-5

Structure of 5565-85-5

Chemical Structure| 5565-85-5

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4.5 *For Research Use Only !

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Product Details of [ 5565-85-5 ]

CAS No. :5565-85-5
Formula : C14H14Sn
M.W : 300.97
SMILES Code : C[Sn]1(C)C2=C(C3=C1C=CC=C3)C=CC=C2
MDL No. :MFCD22581313

Safety of [ 5565-85-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301+H311+H331-H410
Precautionary Statements:P501-P261-P273-P270-P271-P264-P280-P391-P361+P364-P301+P310+P330-P302+P352+P312-P304+P340+P311-P403+P233-P405
Class:6.1
UN#:2788
Packing Group:

Application In Synthesis of [ 5565-85-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5565-85-5 ]

[ 5565-85-5 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 6287-82-7 ]
  • [ 5565-85-5 ]
  • [ 201-69-4 ]
  • 2
  • [ 7657-08-1 ]
  • [ 5565-85-5 ]
  • [ 17825-71-7 ]
  • 3
  • [ 3141-24-0 ]
  • [ 5565-85-5 ]
  • 2-bromophenanthro[9,10-b]thiophene [ No CAS ]
YieldReaction ConditionsOperation in experiment
32% With bis(tri-t-butylphosphine)palladium(0); cesium fluoride; In tetrahydrofuran; at 60℃; for 12h;Inert atmosphere; Under a nitrogen flow <strong>[3141-24-0]2,3,5-tribromothiophene</strong> (20 g, 62.34 mmol), 5,5-dimethyl-5H-dibenzo[b,d]stannole (18.76 g, 62.34 mmol), Pd (PtBu3) 2 (1.59 g, 3.12 mmol), CsF (47.35 g, 311.69 mol) and THF (500 ml) the mixture And it stirred for 12 hours at 60 C. The reaction was terminated by column chromatography and then lower the temperature to room temperature, remove the solvent and then filter the reaction to FlorisilBlood (Hexane: MC = 10: 1 (v / v)) to give 2-bromophenanthro[9,10-b]thiophene (6.25 g, yield 32%).
 

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