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Chemistry
Organic Building Blocks
Aryls
2,3-Dimethoxy-1-naphthaldehyde
Chemistry
Organic Building Blocks
Aryls
Ethers Aldehydes Benzene Compounds

[ CAS No. 56252-09-6 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
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Chemical Structure| 56252-09-6
Chemical Structure| 56252-09-6
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Quality Control of [ 56252-09-6 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification
Alternatived Products of [ 56252-09-6 ]

Product Details of [ 56252-09-6 ]

CAS No. :56252-09-6 MDL No. :MFCD06798095
Formula : C13H12O3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 216.23 Pubchem ID :-
Synonyms :

Safety of [ 56252-09-6 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338+P310 UN#:1759
Hazard Statements:H318 Packing Group:Ⅲ
GHS Pictogram:

Application In Synthesis of [ 56252-09-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 56252-09-6 ]

[ 56252-09-6 ] Synthesis Path-Downstream   1~6

  • 1
  • [ 10103-06-7 ]
  • [ 68-12-2 ]
  • [ 56252-09-6 ]
Reference： [1]Journal of Organic Chemistry,1956,vol. 21,p. 21
  • 2
  • [ 109-72-8 ]
  • [ 10103-06-7 ]
  • [ 56252-09-6 ]
YieldReaction ConditionsOperation in experiment
With N,N,N,N,-tetramethylethylenediamine; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; hexane; N,N-dimethyl-formamide; (a) 2,3-Dimethoxy-naphthalene-1-carbaldehyde n-Butyl lithium in hexane (1.6 N, 31.3 ml) was gradually added to a solution of <strong>[10103-06-7]2,3-dimethoxynaphthalene</strong> (9.4 g) and N,N,N',N'-tetramethylethylenediamine (7.4 ml) in ether (150 ml) under argon at 0 C. The reaction mixture was stirred at room temperature for two hours, cooled to 0 C. and DMF (7.3 g) in ether (20 ml) added. The reaction mixture was stirred at room temperature overnight and poured in ice water. The product was extracted with ether, washed with water, dried, evaporated and recrystallized from ether. Yield: 4.2 g. 1H-NMR (DMSO-d6, 400 MHz): 10.68 (s,1H, CHO), 8.95-8.97 (m, 1H), 7.87-7.89 (m,1H), 7.80 (s,1H), 7.49-7.51 (m,2H), 4.00 (s,6H).
Reference： [1]Patent: US2004/34011,2004,A1
  • 3
  • [ 2879-20-1 ]
  • [ 56252-09-6 ]
  • 1-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-3-(2,3-dimethoxynaphthalen-1-yl)propenone [ No CAS ]
Reference： [1]Chemical Biology and Drug Design,2015,vol. 85,p. 729 - 742
[2]RSC Advances,2015,vol. 5,p. 46330 - 46338
  • 4
  • [ 59576-26-0 ]
  • [ 56252-09-6 ]
  • (E)-3-(2,3-dimethoxynaphthalen-1-yl)-1-(4-methylpyridin-2-yl)prop-2-en-1-one [ No CAS ]
Reference： [1]Angewandte Chemie - International Edition,2016,vol. 55,p. 1401 - 1405
    Angew. Chem.,2016,vol. 128,p. 1423 - 1427,5
  • 5
  • [ 20628-06-2 ]
  • [ 56252-09-6 ]
  • (E)-3-(2,3-dimethoxynaphthalen-1-yl)-1-(2-hydroxy-4,5-dimethoxyphenyl)prop-2-en-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
With potassium hydroxide In ethanol
With potassium hydroxide In ethanol; water at 0 - 20℃; for 24h;
Reference： [1]Koh, Dongsoo; Shin, Soon Young; Sung, Jiha; Ahn, Seunghyun; Lim, Yoongho [Magnetic Resonance in Chemistry, 2017, vol. 55, # 9, p. 856 - 863]
[2]Koh, Dongsoo; Jung, Yearam; Kim, Beom Soo; Ahn, Seunghyun; Lim, Yoongho [Magnetic Resonance in Chemistry, 2016, vol. 54, # 10, p. 842 - 851]
  • 6
  • [ 1535-67-7 ]
  • [ 10103-06-7 ]
  • [ 66920-80-7 ]
  • [ 56252-09-6 ]
YieldReaction ConditionsOperation in experiment
61%; 38% General procedure: In a round-bottomed flask equipped with a stirring bar and rubber septum was placed a 1 M solution of SnCl4 in anhydrous CH2Cl2 (1 mL, 1 mmol). To this solution was added PhSCF2H (1; 240.2 mg, 1.5 mmol) in anhydrous CH2Cl2 (1.5 mL), followed by a solution of an aromatic compound (0.5 mmol) in anhydrous CH2Cl2 (1 mL). The reaction was allowed to proceed for 2 h before it was quenched with a solution of IBX (140 mg, 0.5 mmol) in DMSO/H2O (4 mL; 3:1 v:v). After 2 h of stirring at rt, the reaction mixture was quenched by addition of a saturated aqueous solution of sodium thiosulfate (10 mL), then basified with a saturated aqueous solution of sodium hydrogen carbonate (10 mL), followed by stirring and extraction with CH2Cl2 (3 × 10 mL). The combined organic layers were washed with water (3 × 10 mL) and brine (10 mL), dried (anhydrous MgSO4), filtered and concentrated (aspirator). The residue was purified by PTLC, radial chromatography or column chromatography to furnish analytically pure product.
Reference： [1]Synthesis,2018,vol. 50,p. 2033 - 2040

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