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CAS No. : | 5649-49-0 | MDL No. : | MFCD00144944 |
Formula : | C10H18N2O4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | WCJNJOOLQWJKLU-UHFFFAOYSA-N |
M.W : | 230.26 | Pubchem ID : | 79733 |
Synonyms : |
|
Chemical Name : | 3,3'-(Piperazine-1,4-diyl)dipropanoic acid |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
4.58 g | With sodium hydroxide; at 20℃; | 5 g (25.7 mmol) piperazine.6H2O was dissolved in 140 ml 10% NaOH solution and 8.08 g (52.8 mmol) of 3-bromopropanoic acid was added. The yellow, clear solution was stirred overnight at RT. The solution was acidified with 37% HCl and the product then precipitated as a light yellow crystalline substance. The mixture was stored overnight at 4 C., the precipitate filtered off, washed with water and dried in vacuo. Yield: 4.58 g of light yellow, crystalline substance (MS: calc.: 230.13. found 229.17 [M-H]-) |