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Chemical Structure| 56518-76-4 Chemical Structure| 56518-76-4

Structure of 56518-76-4

Chemical Structure| 56518-76-4

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Product Details of [ 56518-76-4 ]

CAS No. :56518-76-4
Formula : C7H10N4O4
M.W : 214.18
SMILES Code : O=C(OC)NC1=NC(OC)=NC(OC)=N1

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Application In Synthesis of [ 56518-76-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 56518-76-4 ]

[ 56518-76-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 16370-63-1 ]
  • [ 616-38-6 ]
  • [ 56518-76-4 ]
YieldReaction ConditionsOperation in experiment
In tetrahydrofuran; EXAMPLE 5 Methyl (4,6-dimethoxy-1,3,5-triazin-2-yl)carbamate <strong>[16370-63-1]2-Amino-4,6-dimethoxy-1,3,5-triazine</strong> (55.3 g) was added portionwise to 50% sodium hydride (38.0 g) in 1000 ml dry tetrahydrofuran at ambient temperature under nitrogen. After the reaction mixture was stirred for 1.25 hours, dimethylcarbonate (50.0 g) was added dropwise. The reaction mixture was stirred 16 hours at ambient temperature under nitrogen and concentrated hydrochloric acid (68 ml) was slowly added followed by 100 ml tetrahydrofuran. Insoluble material was removed via filtration and discarded. The filtrate was dried and the solvent removed under reduced pressure to give a solid which upon crystallization from ethanol afforded 43.9 g of the tital compound, m.p. 118-122 C.
 

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