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Chemical Structure| 5665-79-2 Chemical Structure| 5665-79-2

Structure of 5665-79-2

Chemical Structure| 5665-79-2

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Product Details of [ 5665-79-2 ]

CAS No. :5665-79-2
Formula : C9H22O2Si
M.W : 190.36
SMILES Code : OCCCCCCO[Si](C)(C)C

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Application In Synthesis of [ 5665-79-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5665-79-2 ]

[ 5665-79-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 38222-83-2 ]
  • [ 5665-79-2 ]
  • 6-Trimethylsiloxy-1-hexyltriflate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With trifluoromethylsulfonic anhydride; In dichloromethane; To a solution of 6-trimethylsiloxy-1-hexanol (11.6 mmol) in dry dichloromethane (50 mL) is added <strong>[38222-83-2]2,6-di-tert-butyl-4-methylpyridine</strong> (4.6 g, 22.2 mmol) and triflic anhydride (3.7 mL, 22.2 mmol) at 0° C. The reaction is stirred at room temperature for 20 min, poured into water, and extracted with dichloromethane. The combined extracts are dried over anhydrous sodium sulfate and concentrated in vacuo and to afford 6-trimethylsiloxy-1-hexyl triflate (40) which is used without further purification.
 

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