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Chemical Structure| 56735-29-6 Chemical Structure| 56735-29-6

Structure of 56735-29-6

Chemical Structure| 56735-29-6

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Product Details of [ 56735-29-6 ]

CAS No. :56735-29-6
Formula : C10H12N4O2
M.W : 220.23
SMILES Code : CC(N/N=C(C1=CC=CC=C1)/C(NN)=O)=O
MDL No. :MFCD28559321

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Application In Synthesis of [ 56735-29-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 56735-29-6 ]

[ 56735-29-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 56735-29-6 ]
  • [ 41394-05-2 ]
YieldReaction ConditionsOperation in experiment
In butan-1-ol; at 20 - 132℃; for 8h;Reflux; Room temperature,The metered butanol was pumped into the cyclone,Stirred into a small amount of catalyst,And then weighing the cake after the last step into the kettle,Jacket through the steam temperature to 132 ,Reflux water separation reaction 8h;After completion of the reaction,Jacket cooling water cooling to room temperature crystallization,The liquid material is put into an enclosed centrifuge to be centrifuged,The filter cake was removed and sent to a rake dryer for drying (60 C)Packaging to be finished metamitron;Drying process of the waste gas condensed collected condensate into the centrifugal mother liquor,Non-condensable gas into the exhaust gas treatment system;Collected centrifugal mother liquor with the cycle of cyclization process,After applying 10 batches,The mother liquor was put into a butanol distillation kettle to carry out atmospheric distillation,Out of the solvent butanol applied,After the distillation,After cooling to cool the residue (Mainly containing HHP, phenazinone) Collect the use of recycling processes.
 

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