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[ CAS No. 575456-77-8 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 575456-77-8
Chemical Structure| 575456-77-8
Structure of 575456-77-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 575456-77-8 ]

CAS No. :575456-77-8 MDL No. :N/A
Formula : - Boiling Point : -
Linear Structure Formula :- InChI Key :AXSCZKAJIQMFGF-UHFFFAOYSA-J
M.W : - Pubchem ID :73162355
Synonyms :

Safety of [ 575456-77-8 ]

Signal Word:Warning Class:
Precautionary Statements:P501-P261-P270-P271-P264-P280-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330-P302+P352+P312-P304+P340+P312 UN#:
Hazard Statements:H302+H312+H332-H315-H319 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 575456-77-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 575456-77-8 ]

[ 575456-77-8 ] Synthesis Path-Downstream   1~4

  • 1
  • [ CAS Unavailable ]
  • [ 310874-13-6 ]
  • [ 575456-77-8 ]
YieldReaction ConditionsOperation in experiment
In chlorobenzene under N2; Rh complex, ligand (9.6 equiv.) and chlorobenzene heated underreflux for 24 h in Soxlet apparatus fitted with thimble contg. dried Na 2CO3 and sand; solvent evapd.; purified by flash chromy. (basic alumina, MeOH);
16 g In chlorobenzene at 130 - 135℃; for 3h; 2 Take a 250mL three-necked flask, and add chlorobenzene (150mL) in sequence under stirring.Compound 2-2 (14.1 g, 45.2 mmol) and dipolyrhodium acetate (5 g, 11.3 mmol); heated to 130 ° C-135 ° C, and reacted at reflux for 3 hours;The three-necked flask is equipped with a vacuum distillation device, and the solvent is distilled while stirring the reaction until it does not drip;Add n-hexane (60 mL), beat, filter, and dry the solid to obtain 16 g of Rh2 {(s) -nttl} 4.
  • 2
  • [ 575456-77-8 ]
  • [ CAS Unavailable ]
  • [ CAS Unavailable ]
  • [ CAS Unavailable ]
YieldReaction ConditionsOperation in experiment
100% In dichloromethane at 20℃; for 0.5h;
  • 3
  • [ 1122-58-3 ]
  • [ 575456-77-8 ]
  • [ CAS Unavailable ]
  • [ CAS Unavailable ]
YieldReaction ConditionsOperation in experiment
100% In dichloromethane at 20℃; for 0.5h;
  • 4
  • [ CAS Unavailable ]
  • [ 310874-13-6 ]
  • [ 575456-77-8 ]
YieldReaction ConditionsOperation in experiment
48% With lithium carbonate In ethanol at 20℃; for 6.5h; Inert atmosphere; Heating;
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