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[ CAS No. 58076-32-7 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Chemical Structure| 58076-32-7
Chemical Structure| 58076-32-7
Structure of 58076-32-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 58076-32-7 ]

CAS No. :58076-32-7 MDL No. :MFCD09809340
Formula : C9H11ClO3S Boiling Point : -
Linear Structure Formula :- InChI Key :LHYZGURMLPSRFU-UHFFFAOYSA-N
M.W :234.70 Pubchem ID :12239196
Synonyms :

Safety of [ 58076-32-7 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3261
Hazard Statements:H302+H312+H332-H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 58076-32-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 58076-32-7 ]

[ 58076-32-7 ] Synthesis Path-Downstream   1~6

  • 2
  • [ 7790-94-5 ]
  • [ 622-85-5 ]
  • [ 58076-32-7 ]
YieldReaction ConditionsOperation in experiment
50% In dichloromethane; for 2h; General procedure: 11a (1.84 g, 17 mmol) was dissolved in DCM (50 mL). Thenchlorosulfonic acid (2.97 g, 25.5 mmol) in DCM (20 mL) was addedover 60 min at -5 C. The mixture was allowed to warm to roomtemperature with stirring additional 60 min. The mixture waspoured into ice water and the organic phase was separated,washed with Na2CO3, NaHCO3, water and saturated brine. It wasfinally dried over anhydrous Na2SO4, filtered and evaporated,affording in 12a (2.11 g, 60%). According to the same proceduredescribed for 13a, 10a (203 mg, 0.7 mmol) was treated with 12a(157 mg, 0.76 mmol) to afford 228 mg (71%) of 13b as a whitesolid. According to the same procedure described for P5, 13b(184 mg, 0.40 mmol) was treated with 16a (155 mg, 0.46 mmol)to afford 173 mg (61%) of P6 as a white solid.
  • 3
  • [ 116797-02-5 ]
  • [ 58076-32-7 ]
  • 4-methyl-1'-((4-propoxyphenyl)sulfonyl)-1,4'-bipiperidine [ No CAS ]
YieldReaction ConditionsOperation in experiment
95% With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃;
  • 4
  • [ 58076-32-7 ]
  • [ 6358-64-1 ]
  • N-(4-chloro-2,5-dimethoxyphenyl)-4-propoxybenzenesulfonamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
65 mg Stage #1: 4-n-propoxy-1-benzenesulfonyl chloride; 4-chloro-2,5-dimethoxy-aniline With triethylamine In dichloromethane at 20℃; Stage #2: With lithium hydroxide monohydrate In tetrahydrofuran; methanol; water at 20℃;
  • 5
  • [ 58076-32-7 ]
  • [ 6358-64-1 ]
  • N-(4-chloro-2,5-dimethoxyphenyl)-4-propoxybenzenesulfonamide [ No CAS ]
  • C26H30ClNO8S2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine In dichloromethane at 20℃;
  • 6
  • [ 58076-32-7 ]
  • [ 2243-61-0 ]
  • 1,4-bis-[(4-n-propoxybenzenesulfonyl)amino]naphthalene [ No CAS ]
YieldReaction ConditionsOperation in experiment
97% With pyridine at 20℃; for 2h;
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