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Chemical Structure| 58358-37-5 Chemical Structure| 58358-37-5

Structure of 58358-37-5

Chemical Structure| 58358-37-5

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Product Details of [ 58358-37-5 ]

CAS No. :58358-37-5
Formula : C12H16O2
M.W : 192.25
SMILES Code : O=C(OCC)CC1=CC(C)=CC=C1C

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Application In Synthesis of [ 58358-37-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 58358-37-5 ]

[ 58358-37-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 13612-34-5 ]
  • [ 58358-37-5 ]
YieldReaction ConditionsOperation in experiment
2.94 g (84%) With sulfuric acid; In ethanol; (i) Ethyl (2,5-dimethylphenyl)acetate A solution of <strong>[13612-34-5](2,5-dimethylphenyl)acetic acid</strong> (3.0 g; 18.3 mmol) and H2SO4 (conc.; 0.1 mL) in EtOH (40 mL) was refluxed over 6 days. The solution was concentrated, ether (40 mL) was added, and the resultant mixture was washed with Na2CO3 solution (2*25 mL) and water (1*25 mL). The organic phase was dried (MgSO4) and evaporated, yielding 2.94 g (84%) of the sub-title compound a clear colourless liquid. Purity 97%. 1H-NMR (400 MHz; CDCl3): delta 7.08 (d, 1H); 7.02 (d, 1H); 7.00 (s, 1H); 4.17 (q, 2H); 3.61 (s, 2H); 2.33 (s, 3H); 2.29 (s, 3H); 1.28 (t, 3H).
  • 2
  • [ 58358-37-5 ]
  • [ 13612-34-5 ]
 

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