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Chemical Structure| 58467-92-8 Chemical Structure| 58467-92-8

Structure of 58467-92-8

Chemical Structure| 58467-92-8

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Product Details of [ 58467-92-8 ]

CAS No. :58467-92-8
Formula : C15H14N2
M.W : 222.29
SMILES Code : C1(N/C=C/C=N/C2=CC=CC=C2)=CC=CC=C1
MDL No. :MFCD00051805

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Application In Synthesis of [ 58467-92-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 58467-92-8 ]

[ 58467-92-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 58467-92-8 ]
  • [ 15666-97-4 ]
  • [ 108-24-7 ]
  • n-octyl (2E,4E)-5-[acetyl(phenyl)amino]-2-cyanopenta-2,4-dienoate [ No CAS ]
YieldReaction ConditionsOperation in experiment
79% at 115℃; for 2h;Inert atmosphere; First Stage: Preparation of n-octyl (2E,4E)-5-[acetyl(phenyl)amino]-2-cyanopenta-2,4-dienoate 3-Anilinoacrolein-aniline (27.7 g, 0.125 mol) and <strong>[15666-97-4]n-<strong>[15666-97-4]octyl cyanoacetate</strong></strong> (26.3 ml, 0.125 mol) are heated in 70 ml of acetic anhydride at 115 C. for 2 hours while bubbling with nitrogen. After cooling, 80 ml of methanol are added and precipitation is allowed to take place. The solid obtained is filtered off and rinsed with methanol. Drying is carried out. 36.4 g of a yellow powder (yield: 79%) of butyl (2E,4E)-5-[acetyl(phenyl)amino]-2-cyanopenta-2,4-dienoate are recovered, which powder is used as is in the following stage.
 

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[ 58467-92-8 ]

Chemical Structure| 58467-94-0

A1191988 [58467-94-0]

N-((1E,3E)-3-(Phenylimino)prop-1-en-1-yl)aniline hydrochloride

Reason: Free-salt