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Chemical Structure| 585-05-7 Chemical Structure| 585-05-7

Structure of 585-05-7

Chemical Structure| 585-05-7

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Product Details of [ 585-05-7 ]

CAS No. :585-05-7
Formula : C3H4N2O4
M.W : 132.07
SMILES Code : O=C(C(O)=O)NC(N)=O

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Application In Synthesis of [ 585-05-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 585-05-7 ]

[ 585-05-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 6270-46-8 ]
  • potassium permanganate [ No CAS ]
  • [ 591-07-1 ]
  • [ 585-05-7 ]
  • 2
  • [ 585-05-7 ]
  • [ 57-13-6 ]
  • [ 2207-75-2 ]
YieldReaction ConditionsOperation in experiment
94.64% At room temperature, 2-carbamido-2-oxoacetic acid (13.20 g, 0.10 mol),Urea (13.81 g, 0.23 mol), p-toluenesulfonic acid (0.086 g, 0.50 mmol),Add ethanol (100mL), heat to 50 C for 6h, cool to 0 C, adjust the pH to 5.5 with an aqueous solution of potassium hydroxide, stir and grow for 2h, suction filter, and filter the cake with cold purified water in order.Wash with cold anhydrous ethanol to obtain oltiracil potassium,Yield 94.64%,Tested by HPLC,Where tR = 14.726min is oltiracil potassium,Purity is 99.965%,The maximum single impurity is 0.012%.
 

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