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Chemistry
Organic Building Blocks
Aryls
Methyl 4-methoxybenzodithioate
Chemistry
Organic Building Blocks
Aryls
Ethers Benzene Compounds

[ CAS No. 5874-09-9 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 5874-09-9
Chemical Structure| 5874-09-9
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COA NMR CNMR HPLC LC-MS

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Product Details of [ 5874-09-9 ]

CAS No. :5874-09-9 MDL No. :
Formula : C9H10OS2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 198.31 Pubchem ID :-
Synonyms :

Safety of [ 5874-09-9 ]

Signal Word: Class:
Precautionary Statements: UN#:
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Application In Synthesis of [ 5874-09-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5874-09-9 ]

[ 5874-09-9 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 5874-09-9 ]
  • [ 61150-58-1 ]
  • [ 1174642-55-7 ]
Reference： [1]Journal of Organic Chemistry,2009,vol. 74,p. 5496 - 5501
  • 2
  • [ 5874-09-9 ]
  • [ 61150-58-1 ]
  • [ 74-88-4 ]
  • [ 1174642-15-9 ]
Reference： [1]Journal of Organic Chemistry,2009,vol. 74,p. 5496 - 5501
  • 3
  • [ 13781-53-8 ]
  • [ 5874-09-9 ]
  • 2-(4-methoxyphenyl)thieno[2,3-b]thiophene-3-carbonitrile [ No CAS ]
YieldReaction ConditionsOperation in experiment
87% General procedure: To a stirring suspension of KOtBu (2.0 mmol) in 1,4-dioxane (5 mL) at 0C, corresponding (het)arylacetonitrile (1a-f, 10a-c) (1.0 mmol) in 1,4-dioxane (2 mL) was added dropwise. After further stirring for 10 minutes, a solution of respective Dithioester (2a-i) (1.0 mmol) in 1,4-dioxane (2 mL) was added to the reaction mixture at 0C, followed by further stirring for 1 h at ambient temperature (monitored by TLC). Iodine (506 mg, 2.0 mmol) was added and the reaction mixture was heated at 90C with continuous stirring (monitored by TLC). It was then diluted with 10% aq. Na2S2O3 solution (50 mL) and extracted with EtOAc (3x25 mL), and the combined organic layer was washed with water (3x25 mL) and brine (1x25 mL), dried (anhyd. Na2SO4), and concentrated under reduced pressure. The crude products were purified by silica gel column chromatography using EtOAc/hexane as eluent.
Reference： [1]Tetrahedron Letters,2017,vol. 58,p. 4577 - 4582

Tags: 5874-09-9 synthesis path| 5874-09-9 SDS| 5874-09-9 COA| 5874-09-9 purity| 5874-09-9 application| 5874-09-9 NMR| 5874-09-9 COA| 5874-09-9 structure

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Technical Information

• Benzylic Oxidation • Birch Reduction • Blanc Chloromethylation • Friedel-Crafts Reaction • Hydrogenolysis of Benzyl Ether • Nomenclature of Ethers • Preparation of Alkylbenzene • Preparation of Ethers • Reactions of Benzene and Substituted Benzenes • Reactions of Ethers • Vilsmeier-Haack Reaction
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