Home Cart Sign in  
Chemical Structure| 58824-53-6 Chemical Structure| 58824-53-6

Structure of 58824-53-6

Chemical Structure| 58824-53-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 58824-53-6 ]

CAS No. :58824-53-6
Formula : C9H9ClO
M.W : 168.62
SMILES Code : C=CC(C1=CC=CC(Cl)=C1)O

Safety of [ 58824-53-6 ]

Application In Synthesis of [ 58824-53-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 58824-53-6 ]

[ 58824-53-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 2905-65-9 ]
  • [ 1826-67-1 ]
  • [ 58824-53-6 ]
YieldReaction ConditionsOperation in experiment
61% General procedure: To a solution of ethyl benzoate (0.14 g, 1.0 mmol) in THF (10 mL) was slowly added LDBBA (2.4 mL, 0.5 M in THF-hexane, 1.2 mmol) and the mixture was stirring for 3 h at 0 C. To this was slowly added n-butylmagnesium chloride (0.94 mL, 1.6 M in Et2O, 1.5 mmol). After being stirred for 30 min at room temperature, the reaction mixture was quenched with aqueous 1 N HCl (10 mL) and extracted with diethyl ether (2 × 10 mL). The combined organic layers were dried over MgSO4 and filtered. After the removal of solvents in vacuo, purification of the residue by column chromatography on silica gel gave 1-phenylpentan-1-ol (108 mg, 66%). All products in this Letter were confirmed by comparison with data reported in the literatures.5
  • 2
  • [ 221044-05-9 ]
  • [ 58824-53-6 ]
  • 1-(3-chlorophenyl)-3-(1-(pyrimidin-2-yl)-1H-indol-2-yl)propan-1-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; In water; at 80℃; for 12h;Schlenk technique; Green chemistry; General procedure: Heterocycles 1 (0.2mmol, 1.0 equiv), allylic alcohols 2 (0.4 mmol, 2.0 equiv), [Cp*RhCl2]2 (2.5mol %), AgSbF6 (0.02mmol, 10mol %) and H2O (2mL) were charged into a Schlenk tube under air. The reaction mixture was stirred for 12hat 80C. After the reaction was complete, the mixture was extracted with CH2Cl2 three times. The combined organic layer was dried with anhydrous Na2SO4 and evaporated in vacuum. The crude product was purified by flash chromatography on silica gel using hexane/ethyl acetate as the eluent to give the pure product 3.
 

Historical Records