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poly(N-ethylacrylamide), product of emulsion polymerization in presence of 10 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) and 1 wt percent 2,2\-azobisisobutyronitrile; monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 1 wt percent 2,2\-azobisisobutyronitrile, 5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) at 352 bar; monomer(s): N-ethylacrylamide, 10 percent w/v[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 2 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) and 1 wt percent 2,2\-azobisisobutyronitrile; monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 0.5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) and 2,2\-azobisisobutyronitrile; monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 0.2 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) and 1 wt percent 2,2\-azobisisobutyronitrile; monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), polymerization product in presence of 10 wt percent poly(3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate); monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 0.5 wt percent 2,2\-azobisisobutyronitrile and 5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate); monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 2.0 wt percent 2,2\-azobisisobutyronitrile, 5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate); monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 1 wt percent 2,2\-azobisisobutyronitrile, 5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate); monomer(s): N-ethylacrylamide, 20 percent w/v[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 1 wt percent 2,2\-azobisisobutyronitrile, 5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate); monomer(s): N-ethylacrylamide, 30 percent w/v[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 1 wt percent 2,2\-azobisisobutyronitrile, 5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) at pressure 276 bar; monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of emulsion polymerization in presence of 1 wt percent 2,2\-azobisisobutyronitrile, 5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) at pressure 428 bar; monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of polymerization in presence of 10 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) and bis[2-(perfluorooctyl)ethyl] 4,4-azobis(4-cyanopentanoate); monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of polymerization in presence of 5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) and bis[2-(perfluorooctyl)ethyl] 4,4-azobis(4-cyanopentanoate); monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of polymerization in presence of 2 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate) and bis[2-(perfluorooctyl)ethyl] 4,4-azobis(4-cyanopentanoate); monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of polymerization in presence of 0.5 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate), bis[2-(perfluorooctyl)ethyl] 4,4-azobis(4-cyanopentanoate); monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of polymerization in presence of 0.2 wt percent poly(3-O-methacryloyl-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate), bis[2-(perfluorooctyl)ethyl] 4,4-azobis(4-cyanopentanoate); monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), prepared in presence of poly(3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-D-glucofuranose)-b-poly(1,1-dihydroperfluorooctyl methacrylate), bis[2-(perfluorooctyl)ethyl] 4,4-azobis-4-cyanopentanoate; monomer(s): N-ethylacrylamide[ No CAS ]
poly(N-ethylacrylamide), product of polymerization in presence of bis[2-(perfluorooctyl)ethyl] 4,4-azobis(4-cyanopentanoate) and in absence of surfactant; monomer(s): N-ethylacrylamide[ No CAS ]
In methanol; at 140℃; for 0.5h;Microwave irradiation;
General procedure: A solution of N-methylacrylamide (2) (1.88 g, 22.0 mmol) and cyclopentylamine (1.98 mL, 20.0 mmol) in MeOH (14 mL) was heated under microwave irradiation to 140 C for 30 min (Biotage Initiator). The volatiles were removed under reduced pressure, the residue diluted with MeOH (20 mL) and purified by strong cation exchange filtration (50 g SCX-2 cartridge) washing with MeOH (100 mL) and eluting with 7 M methanolic NH3 (100 mL). The eluted product was concentrated under reduced pressure to afford the title compound 3 as a brown oil (3.09 g, 18.2 mmol, 91%). This was used directly with no further purification.