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Chemical Structure| 59755-25-8 Chemical Structure| 59755-25-8

Structure of 59755-25-8

Chemical Structure| 59755-25-8

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Product Details of [ 59755-25-8 ]

CAS No. :59755-25-8
Formula : C9H9NO2
M.W : 163.17
SMILES Code : CC(NC1=CC=CC(C=O)=C1)=O
MDL No. :MFCD00066303
InChI Key :KBKWZUVMKBNTFP-UHFFFAOYSA-N
Pubchem ID :256849

Safety of [ 59755-25-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 59755-25-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 59755-25-8 ]

[ 59755-25-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6398-87-4 ]
  • [ 75-36-5 ]
  • N-[3-(1,3-dioxolan-2-yl)phneyl]acetamide [ No CAS ]
  • [ 59755-25-8 ]
YieldReaction ConditionsOperation in experiment
85% With pyridine; In ethyl acetate; Pyridine (31.3 g, 0.4 mole) was added to the above cooled (ice bath) ethylacetate solution of 2-(3-aminophenyl)1,3-dioxolane followed by dropwise addition of acetyl chloride (31.1 g, 0.4 mole) in ethyl acetate (50 mL) over 45 minutes. The ice bath was removed and the mixture stirred at room temperature for 30 minutes before being washed with water and dried over magnesium sulfate. Evaporation of the solvent afford N-[3-(1,3-dioxolan-2-yl)phneyl]acetamide (58.2 g, 85%) as an amber oil used without further purification below. Step (d) N-(3-Formylphenyl)acetamide
 

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Technical Information

• Acyl Group Substitution • Barbier Coupling Reaction • Baylis-Hillman Reaction • Benzylic Oxidation • Birch Reduction • Blanc Chloromethylation • Bucherer-Bergs Reaction • Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions • Chan-Lam Coupling Reaction • Clemmensen Reduction • Complex Metal Hydride Reductions • Corey-Chaykovsky Reaction • Corey-Fuchs Reaction • Fischer Indole Synthesis • Friedel-Crafts Reaction • Grignard Reaction • Hantzsch Dihydropyridine Synthesis • Henry Nitroaldol Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Hydrogenolysis of Benzyl Ether • Julia-Kocienski Olefination • Knoevenagel Condensation • Lawesson's Reagent • Leuckart-Wallach Reaction • Mannich Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Mukaiyama Aldol Reaction • Nozaki-Hiyama-Kishi Reaction • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Alkylbenzene • Preparation of Amines • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reformatsky Reaction • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Carbodiimides and Related Reagents • Specialized Acylation Reagents-Ketenes • Specialized Acylation Reagents-Vilsmeier Reagent • Stetter Reaction • Stobbe Condensation • Tebbe Olefination • Ugi Reaction • Vilsmeier-Haack Reaction • Wittig Reaction • Wolff-Kishner Reduction

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