[ CAS No. 602-56-2 ]

{[proInfo.proName]}
Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 602-56-2
Chemical Structure| 602-56-2
Structure of 602-56-2

Quality Control of [ 602-56-2 ]

Purity: {[proInfo.showProBatch.pb_purity]}

Related Doc. of [ 602-56-2 ]

SDS

Product Details of [ 602-56-2 ]

CAS No. :602-56-2MDL No. :MFCD00092562
Formula :C19H13NBoiling Point :411.1°C at 760 mmHg
Linear Structure Formula :-InChI Key :MTRFEWTWIPAXLG-UHFFFAOYSA-N
M.W :255.31Pubchem ID :69041
Synonyms :

Computed Properties of [ 602-56-2 ]

TPSA : 12.9 H-Bond Acceptor Count : 1
XLogP3 : 5.2 H-Bond Donor Count : 0
SP3 : 0.00 Rotatable Bond Count : 1

Safety of [ 602-56-2 ]

Signal Word:WarningClassN/A
Precautionary Statements:P261-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 602-56-2 ]

  • Downstream synthetic route of [ 602-56-2 ]

[ 602-56-2 ] Synthesis Path-Downstream   1~10

  • 1
  • 9-trifluoromethanesulphonyloxyacridine trifluoromethanesulphonic acid salt [ No CAS ]
  • [ 98-80-6 ]
  • [ 602-56-2 ]
  • 2
  • [ 10228-92-9 ]
  • [ 98-80-6 ]
  • [ 602-56-2 ]
  • 3
  • [ 4357-57-7 ]
  • [ 98-80-6 ]
  • [ 602-56-2 ]
  • 4
  • [ 1207-69-8 ]
  • [ 98-80-6 ]
  • [ 602-56-2 ]
YieldReaction ConditionsOperation in experiment
96.8% With tetrakis(triphenylphosphine) palladium(0); sodium carbonate; In water; toluene; at 40℃; for 3h; In a 250 mL three-necked flask, 21.4 g (0.1 mol) of 9-chloroacridine, 14.6 g (0.12 mol) of phenylboronic acid, 0.11 g of Pd (PPh3) 4 catalyst, 100 g of toluene, 2 g of sodium carbonate, and 18 g of deionized water were sequentially added. , Heated to 40 C., reacted for 3 hours, cooled to 25 C., removed the solvent by rotary evaporation, washed with 100 g of methanol and dispersed, and filtered to obtain a crude product. The crude product was purified with 80 g of toluene and dried to obtain 24.7 g of the product, a yield of 96.8%. HPLC The content is 99.65%.
  • 5
  • [ 108-86-1 ]
  • acridin-9-ylboronic acid [ No CAS ]
  • [ 602-56-2 ]
  • 6
  • [ 116465-43-1 ]
  • [ 602-56-2 ]
  • ammonium chloride [ No CAS ]
  • [ 537-67-7 ]
  • [ 100-47-0 ]
  • 7
  • [ 591-50-4 ]
  • [ 2835-77-0 ]
  • [ 602-56-2 ]
  • 8
  • [ 4051-56-3 ]
  • ZnCl2 [ No CAS ]
  • [ 602-56-2 ]
  • 9
  • [ 122-39-4 ]
  • [ 65-85-0 ]
  • [ 602-56-2 ]
YieldReaction ConditionsOperation in experiment
65% With phthalic acid dimethyl ester; zinc(II) chloride; at 100℃; for 2h;Microwave irradiation; A mixture of dimethyl phthalate (20 mmol), diphenylamine (10 mmol), benzoic acid( 10 mmol) and zinc chloride (20 mmol) was stirred and microwave irradiated at 100 C and 120 W for 2 h. The mixture was diluted with dichloromethane, washed with water, diluted with sodium hydroxide, washed again with water and dried over magnesium sulphate. After evaporationof the solvent, the crude product was recrystallised from toluene/ethanol. Yield 65%; the % of elements found/calculated, C 89.42/89.38, H 5.10/5.13, N 5.48/5.49; 1H NMR (CDCl3), delta, ppm (J, Hz): 7.21 (1H, m); 7.39 (2H,m); 7.42 (2H, m); 7.57 (2H, m); 7.69 (2H, dd, J = 11.8); 7.74 (2H, m), 8.28 (2H, dd, J = 11.8).
  • 10
  • [ 140-10-3 ]
  • [ 122-39-4 ]
  • [ 5435-44-9 ]
  • [ 602-56-2 ]
Related Products
Historical Records

Related Functional Groups of
[ 602-56-2 ]

Aryls

Chemical Structure| 3558-69-8

[ 3558-69-8 ]

2,6-Diphenylpyridine

Similarity: 0.91

Chemical Structure| 605-03-8

[ 605-03-8 ]

4-Phenylquinoline

Similarity: 0.86

Chemical Structure| 1203578-65-7

[ 1203578-65-7 ]

7-Bromo-2-phenylquinoline

Similarity: 0.80

Chemical Structure| 178265-65-1

[ 178265-65-1 ]

4-([2,2':6',2''-Terpyridin]-4'-yl)aniline

Similarity: 0.77

Chemical Structure| 1498333-87-1

[ 1498333-87-1 ]

(4-(Pyridin-2-yl)phenyl)methanamine hydrochloride

Similarity: 0.76

Related Parent Nucleus of
[ 602-56-2 ]

Aromatic Heterocycles

Chemical Structure| 611-64-3

[ 611-64-3 ]

9-Methylacridine

Similarity: 0.98

Chemical Structure| 581-28-2

[ 581-28-2 ]

Acridin-2-amine

Similarity: 0.95

Chemical Structure| 90-45-9

[ 90-45-9 ]

9-Aminoacridine

Similarity: 0.90

Chemical Structure| 1198-37-4

[ 1198-37-4 ]

2,4-Dimethylquinoline

Similarity: 0.89

Chemical Structure| 605-03-8

[ 605-03-8 ]

4-Phenylquinoline

Similarity: 0.86

Other Aromatic Heterocycles

Chemical Structure| 611-64-3

[ 611-64-3 ]

9-Methylacridine

Similarity: 0.98

Chemical Structure| 581-28-2

[ 581-28-2 ]

Acridin-2-amine

Similarity: 0.95

Chemical Structure| 90-45-9

[ 90-45-9 ]

9-Aminoacridine

Similarity: 0.90

Chemical Structure| 904886-12-0

[ 904886-12-0 ]

Benzo[h]quinoline-2-carbaldehyde

Similarity: 0.80

Chemical Structure| 18123-20-1

[ 18123-20-1 ]

Acridin-4-ol

Similarity: 0.77

Acridinium Series

Chemical Structure| 611-64-3

[ 611-64-3 ]

9-Methylacridine

Similarity: 0.98

Chemical Structure| 581-28-2

[ 581-28-2 ]

Acridin-2-amine

Similarity: 0.95

Chemical Structure| 90-45-9

[ 90-45-9 ]

9-Aminoacridine

Similarity: 0.90

Chemical Structure| 18123-20-1

[ 18123-20-1 ]

Acridin-4-ol

Similarity: 0.77

Chemical Structure| 1207-69-8

[ 1207-69-8 ]

9-Chloroacridine

Similarity: 0.74