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Chemical Structure| 60373-70-8 Chemical Structure| 60373-70-8

Structure of 60373-70-8

Chemical Structure| 60373-70-8

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Product Details of [ 60373-70-8 ]

CAS No. :60373-70-8
Formula : C9H10O2
M.W : 150.17
SMILES Code : CCC1=CC=C(OCO2)C2=C1
MDL No. :MFCD00210444

Safety of [ 60373-70-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 60373-70-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 60373-70-8 ]

[ 60373-70-8 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 60373-70-8 ]
  • [ 1180-71-8 ]
  • N-(benzo[d][1,3]dioxol-5-ylmethyl)-2-((1S,3aS,4aR,4bR,9aR,11aS)-1-(furan-3-yl)-9a-(hydroxymethyl)-4b,7,7,11a-tetramethyl-3,5-dioxotetradecahydroisobenzofuro[5,4-f]oxireno[2,3-d]isochromen-9-yl)acetamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
78% With montmorillonite K-10; In ethanol; at 80℃; for 0.5h;Sealed tube; Microwave irradiation; General procedure: To a solution of 1 (2.0 mmol) in absolute EtOH (8.0 mL)in a glass tube was added dropwise the appropriate amine(3.6 mmol) and K-10 (0.3 g mmol-1); the quartz tubewas sealed with reaction mixture and introduced intoa microwave oven. The flask was irradiated for 30 min(150 W) the temperature of 80 C. After completion of thereaction the mixture was filtered, the organic phase wasdried with Na2SO4, filtered and the solvent was evaporatedunder reduced pressure to give the crude products. All thecompounds were purified by column chromatographyon silica gel using 2-5% EtOH-CH2Cl2 as eluent to giveanalytically pure products 3a-m. The products werecharacterized by corresponding spectroscopic data (1H and13C NMR, and HRMS).
 

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