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[ CAS No. 608515-16-8 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 608515-16-8
Chemical Structure| 608515-16-8
Chemical Structure| 608515-16-8
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Product Details of [ 608515-16-8 ]

CAS No. :608515-16-8 MDL No. :MFCD09260785
Formula : C11H17N Boiling Point : -
Linear Structure Formula :- InChI Key :JPETYCDJGPTICO-UHFFFAOYSA-N
M.W : 163.26 Pubchem ID :8167069
Synonyms :

Safety of [ 608515-16-8 ]

Signal Word:Danger Class:8
Precautionary Statements:P301+P330+P331-P303+P361+P353-P363-P304+P340-P310-P321-P260-P264-P280-P305+P351+P338-P405-P501 UN#:2735
Hazard Statements:H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 608515-16-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 608515-16-8 ]

[ 608515-16-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 154532-34-0 ]
  • [ 608515-16-8 ]
YieldReaction ConditionsOperation in experiment
With ammonia; hydrogen;nickel; In water; at 40℃; c) 3-tert-Butyl-benzylamineA mixture of 0.84 g (5.1 mmol) of <strong>[154532-34-0]3-tert-butyl-benzonitrile</strong>, 1 ml of 25 % aq. NH3 and 0.1 g of Raney-Nickel is hydrogenated at 400C. After the completion of the reaction, the catalyst is filtered off and washed with MeOH. The filtrate is evaporated in vacuo, and the residue is purified by chromatography on silica gel (DCM/MeOH 90/10) to give the product in the form of a green oil.HPLC (Nucleosil 100-3 C18HD, 4 x 70 mm, 3 mum, 1.0 ml/min, 20-100 % AcCN/H2O/6 min, 100 % AcCN/1.5 min, 100-20 % AcCN/H2O/0.5 min) retention time: 2.81 min. Rf (hexane/EtOAc = 95/5): 0.26.MS (ES+): 164 = [M+H]+.1H-NMR (400 MHz, CDCI3): 7.40-7.33 (m, 3H), 7.20-7.18 (m, 1H), 3.90 (s, 2H), 1.60 (bs, 2H), 1.39 (s, 9H).
With ammonia; hydrogen;nickel; In water; at 40℃; A mixture of 0.84 g (5.1 mmol) <strong>[154532-34-0]3-tert-butyl-benzonitrile</strong>, 1 mL (25% aq. NH3) and 0.1 g Raney-Nickel is hydrogenated at 40 C. After completion of reaction, the catalyst is filtered off and washed with MeOH. The solvent is removed in vacuo and the residue is purified by chromatography on silica gel (DCM/MeOH 90/10) to give 0.84 g of the desired product as a green oil.tR (HPLC, Nucleosil C18 column, 20-100% CH3CN/H2O/6 min, 100% CH3CN/1.5 min, 100-20% CH3CN/H2O/0.5 min, flow: 1.0 ml/min): 2.81 min.Rf: (hexane/AcOEt=95/5): 0.26MS (ES+): 164=[M+H]+ 1H-NMR (400 MHz, CDCl3): 7.40-7.33 (m, 3H), 7.20-7.18 (m, 1H), 3.90 (s, 2H), 1.60 (bs, 2H), 1.39 (s, 9H).
With ammonia; hydrogen;nickel; In methanol; water; under 2585.81 Torr; for 2h; To 3-te/t-butylbenzonitrile (400 mg) in MeOH (5 mL), aqueous ammonium hydroxide (ImL) and Raney Nickel (catalytic) were added and the reaction mixture was hydrogenated at 50psi for 2h. Then the reaction mixture was filtered and solvent evaporated. (3-te/t-butylphenyl)methanamine was used without any purification.
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