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Chemical Structure| 61001-06-7 Chemical Structure| 61001-06-7

Structure of 61001-06-7

Chemical Structure| 61001-06-7

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Product Details of [ 61001-06-7 ]

CAS No. :61001-06-7
Formula : C17H11BrN2
M.W : 323.19
SMILES Code : BrC1=CC=C(C2=CN(C=CC3=C4C=CC=C3)C4=N2)C=C1

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Application In Synthesis of [ 61001-06-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 61001-06-7 ]

[ 61001-06-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 867044-28-8 ]
  • [ 61001-06-7 ]
  • [ 1027074-37-8 ]
YieldReaction ConditionsOperation in experiment
70% With potassium carbonate;tetrakis(triphenylphosphine) palladium(0); In tetrahydrofuran; water; SYNTHESIS EXAMPLE 3; Synthesis of Compound 7; Compound 7 was synthesized through Reaction Scheme 3 below: Compound 7 was prepared in the same manner as in Synthesis Example 1, except that Intermediate 7d was used instead of Intermediate 1d. Intermediate 7d was obtained using 1-aminoisoquinoline instead of 2-aminopyridine. 10 g of Intermediate 1c (21.08 mmol) and 6.19 g of Intermediate 7d (19.16 mmol) were subjected to a Suzuki reaction, yielding 9.03 g of Compound 7 in the form of a pale yellow powder (yield 70%) (1H NMR (400 MHz, CDCl3) 8.69 (1H), 8.12 (2H), 8.07-8.02 (5H), 7.99-7.95 (4H), 7.89-7.84 (2H), 7.79-7.75 (3H), 7.71-7.65 (4H), 7.64-7.54 (8H), 7.33 (2H), 7.02 (1H)).
 

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