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Chemical Structure| 62390-82-3 Chemical Structure| 62390-82-3

Structure of 62390-82-3

Chemical Structure| 62390-82-3

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Product Details of [ 62390-82-3 ]

CAS No. :62390-82-3
Formula : C16H17N3O2
M.W : 283.33
SMILES Code : O=[N+](C=C(NCC1=CC=CC=C1)NCC2=CC=CC=C2)[O-]
MDL No. :MFCD00214715

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Application In Synthesis of [ 62390-82-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 62390-82-3 ]

[ 62390-82-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 62390-82-3 ]
  • [ 5147-80-8 ]
  • 3-cyano-1-(benzyl)-6-(benzylamino)-2-imino-4-(methylthio)-5-nitropyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
85% With caesium carbonate; In acetonitrile; at 70℃; for 2h; Was added 25 mL round bottom flask N, N'- bis-benzyl amino-2-nitroethylene (1mmol, 283mg), Cs 2CO3(1mmol, 325mg) and 2- (bis (methylthio) methylene) malononitrile (2mmol, 340mg), was added acetonitrile solvent (15mL) was heated to magnetic stirring at 70degeC . The reaction was monitored by TLC, the reaction 2h, complete disappearance of the spot of the material, with the reaction solution was extracted with ethyl acetate, the organic layer was then dried over anhydrous Na2SO4Dried, concentrated to dryness after the drying of the liquid, was then concentrated to dryness on recrystallized (acetone: petroleum ether = 1: 15) to give the yellow solid, dried under an infrared lamp to give the product as a yellow solid, was dried under an infrared lamp product 1-phenyl-6- (benzylamino) -2-imino-4- (methylthio) -5-nitro-1,2-dihydro-pyridine-3-carbonitrile (compound 3) yield 85%.
 

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