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Chemical Structure| 6315-19-1 Chemical Structure| 6315-19-1

Structure of 6315-19-1

Chemical Structure| 6315-19-1

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Product Details of [ 6315-19-1 ]

CAS No. :6315-19-1
Formula : C12H10O2
M.W : 186.21
SMILES Code : O=C(O)C1=C2C=CC(C)=CC2=CC=C1
MDL No. :MFCD00092712

Safety of [ 6315-19-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 6315-19-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6315-19-1 ]

[ 6315-19-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6315-19-1 ]
  • [ 116530-22-4 ]
YieldReaction ConditionsOperation in experiment
Preparation 79: 6-Methylnaphthalen-l-ylamine6-Methylnaphthalene-l-carboxylic acid (2.5Og, 13.4mmol) was mixed with polyphosphoric acid (~50mL) and hydroxylamine hydrochloride (990mg, 14.2mmol). The mixture was heated to 8O0C and stirred for 30min. The temperature was slowly raised to 16O0C (froth.) and the stirring was continued for lhr before the hot solution was added to a water/ice mixture (~1.5L). The resulting solution was washed with EtOAc (20OmL) and then made alkaline with solid NaOH. Extraction with EtOAc (3 x 30OmL), washing of the combined extracts with water (20OmL) and brine (20OmL), drying (MgSO4) and concentration in vacuo afforded the title compound, delta? (DMSO): 2.44 (3H, s), 5.63 (2H, br s), 6.60 (IH, d), 7.01 (IH, d), 7.16 (IH, dd), 7.20 (IH, d), 7.50 (IH, s), 7.97 (IH, d); m/z (ES+) = 158.12 [M+H]+;
 

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