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Chemical Structure| 63285-53-0
Chemical Structure| 63285-53-0
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Product Details of [ 63285-53-0 ]

CAS No. :63285-53-0 MDL No. :MFCD29049605
Formula : C11H9N5 Boiling Point : -
Linear Structure Formula :- InChI Key :WEHSLQMKHNECMN-UHFFFAOYSA-N
M.W : 211.22 Pubchem ID :5323619
Synonyms :

Safety of [ 63285-53-0 ]

Signal Word:Warning Class:
Precautionary Statements:P264-P280-P302+P352-P305+P351+P338-P332+P313-P337+P313-P362 UN#:
Hazard Statements:H315-H319 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 63285-53-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 63285-53-0 ]

[ 63285-53-0 ] Synthesis Path-Downstream   1~83

  • 1
  • [ 63285-53-0 ]
  • [ 116156-98-0 ]
  • [ 138785-68-9 ]
  • [ 138785-69-0 ]
  • 2
  • [ 63285-43-8 ]
  • [ 63285-53-0 ]
  • 4
  • 2-[1-(4-(bromomethyl)benzyl)-1H-pyrazol-3-yl]pyridine [ No CAS ]
  • [ 63285-53-0 ]
  • [ 862538-23-6 ]
  • 5
  • [ 1129-30-2 ]
  • [ 63285-53-0 ]
  • 6
  • [ 63285-53-0 ]
  • iron(II) perchlorate hexahydrate [ No CAS ]
  • (iron(II)(2,6-bis(pyrazol-3-yl)pyridine)2)(ClO4)2*3H2O [ No CAS ]
  • 7
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • sodium perchlorate [ No CAS ]
  • (iron(II)(2,6-bis(pyrazol-3-yl)pyridine)2)(ClO4)2*H2O [ No CAS ]
  • 8
  • [ 63285-53-0 ]
  • nickel(II) perchlorate hexahydrate [ No CAS ]
  • (nickel(II)(2,6-bis(pyrazol-3-yl)pyridine)2)(ClO4)2*2H2O [ No CAS ]
  • 9
  • [ 63285-53-0 ]
  • iron(II) tetrafluoroborate hexahydrate [ No CAS ]
  • (iron(II)(2,6-bis(pyrazol-3-yl)pyridine)2)(BF4)2*2H2O [ No CAS ]
  • 10
  • [ 63285-53-0 ]
  • iron(II) tetrafluoroborate [ No CAS ]
  • [ 111994-63-9 ]
  • 11
  • [ 63285-53-0 ]
  • cobalt(II) chloride hexahydrate [ No CAS ]
  • CoCl2(2,6-bis(pyrazol-3-yl)pyridine) * 0.5 H2O [ No CAS ]
  • 12
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • manganese(II) chloride tetrahydrate [ No CAS ]
  • [ 2926-30-9 ]
  • Fe(2+)*2NC5H3(C3H3N2)2*2CF3SO3(1-)*3H2O=[Fe(NC5H3(C3H3N2)2)2](CF3SO3)2*3H2O#dotMn(2+) [ No CAS ]
  • 13
  • [ 17084-13-8 ]
  • [ 63285-53-0 ]
  • gadolinium(III) chloride hexahydrate [ No CAS ]
  • Gd(C11H9N5)3(3+)*3PF6(1-) = [Gd(C11H9N5)3](PF6)3 [ No CAS ]
  • 14
  • [ 17084-13-8 ]
  • [ 63285-53-0 ]
  • holmium(III) chloride hexahydrate [ No CAS ]
  • Ho(C11H9N5)3(3+)*3PF6(1-) = [Ho(C11H9N5)3](PF6)3 [ No CAS ]
  • 15
  • [ 17084-13-8 ]
  • [ 63285-53-0 ]
  • europium(III) chloride hexahydrate [ No CAS ]
  • Eu(C11H9N5)3(3+)*3PF6(1-) = [Eu(C11H9N5)3](PF6)3 [ No CAS ]
  • 16
  • [ 17084-13-8 ]
  • [ 63285-53-0 ]
  • terbium(III) chloride hexahydrate [ No CAS ]
  • Tb(C11H9N5)3(3+)*3PF6(1-) = [Tb(C11H9N5)3](PF6)3 [ No CAS ]
  • 17
  • [ 63285-53-0 ]
  • iron(II) perchlorate hexahydrate [ No CAS ]
  • potassium tris(oxalato)chromate(III) [ No CAS ]
  • [ 7732-18-5 ]
  • di[bis(2,6-bis(pyrazol-3-yl)pyridine)iron(II)] tris(oxalato)chromate(III) perchlorate pentahydrate [ No CAS ]
  • 18
  • [ 63285-53-0 ]
  • potassium tris(oxalato)chromate(III) [ No CAS ]
  • nickel(II) perchlorate hexahydrate [ No CAS ]
  • [ 7732-18-5 ]
  • di[bis(2,6-bis(pyrazol-3-yl)pyridine)nickel(II)] tris(oxalato)chromate(III) perchlorate hexahydrate [ No CAS ]
  • 19
  • [ 63285-53-0 ]
  • silver tris(oxalato)chromate(III) [ No CAS ]
  • [ 7732-18-5 ]
  • cobalt(II) perchlorate hexahydrate [ No CAS ]
  • di[bis(2,6-bis(pyrazol-3-yl)pyridine)cobalt(II)] tris(oxalato)chromate(III) perchlorate hexahydrate [ No CAS ]
  • 20
  • [ 63285-53-0 ]
  • disodium pentacyanonitrosylferrate(II) dihydrate [ No CAS ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • [Fe(2,6-bis(pyrazol-3-yl)pyridine)2][Fe(CN)5(NO)] [ No CAS ]
  • 21
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • [ 33454-82-9 ]
  • bis(2,6-bis(pyrazol-3-yl)pyridine)iron(II) triflate trihydrate [ No CAS ]
  • 22
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • bariumdioxalatodipyridylchromate(III) * 3 H2O [ No CAS ]
  • [iron(II) bis(2,6-bis(pyrazol-3-yl)pyridine) chromium(III)(2,2'-bipyridine) dioxalate] dihydrate [ No CAS ]
  • 23
  • [ 63285-53-0 ]
  • ammonium hexafluorophosphate [ No CAS ]
  • [ 10049-08-8 ]
  • potassium nitrate [ No CAS ]
  • [Ru(2,6-bis(pyrazol-3-yl)pyridine)2][NO3]2 [ No CAS ]
  • [Ru(2,6-bis(pyrazol-3-yl)pyridine)2][PF6]2 [ No CAS ]
  • 24
  • [ 67-56-1 ]
  • [ 63285-53-0 ]
  • manganese(II) chloride tetrahydrate [ No CAS ]
  • iron(II) perchlorate monohydrate [ No CAS ]
  • K3Cr(oxalate)3*3H2O*Ag3Cr(oxalate)3*3H2O [ No CAS ]
  • [Fe(2,6(bis(pyrazol-3-yl)pyridine)2][MnCr(oxalate)3]2*2,6(bis(pyrazol-3-yl)pyridine)*CH3OH [ No CAS ]
  • 25
  • [ 67-56-1 ]
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • Ba[Cr(1,10-phenanthroline)(oxalate)2]2*3H2O [ No CAS ]
  • [Fe(2,6-bis(pyrazol-3-yl)pyridine)2][Cr(1,10-phenanthroline)(oxalate)2]2*5.5H2O*2.5CH4O [ No CAS ]
  • [Fe(2,6-bis(pyrazol-3-yl)pyridine)2][Cr(1,10-phenanthroline)(oxalate)2]2*0.5H2O*0.5CH4O [ No CAS ]
  • 26
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • potassium bis(oxalato)platinate(II) dihydrate [ No CAS ]
  • [ 940348-55-0 ]
  • 27
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • bariumdioxalatodipyridylchromate(III) * 3 H2O [ No CAS ]
  • [Fe(2,6-bis(pyrazol-3-yl)pyridine)2][Cr(2,2'-bipyridine)(oxalate)2]2*2H2O [ No CAS ]
  • 28
  • [ 63285-53-0 ]
  • cobalt(II) sulphate heptahydrate [ No CAS ]
  • bariumdioxalatodipyridylchromate(III) * 3 H2O [ No CAS ]
  • [Co(2,6-bis(pyrazol-3-yl)pyridine)2][Cr(2,2'-bipyridine)(oxalate)2]2*2H2O [ No CAS ]
  • 29
  • [ 67-56-1 ]
  • [ 63285-53-0 ]
  • [ 553-26-4 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • [ 333-20-0 ]
  • bis[2,6-bis(3-pyrazolyl)pyridine]-4,4'-bipyridinetetrathiocyanatodiiron(II)*CH3OH [ No CAS ]
  • 30
  • [ 63285-53-0 ]
  • iron(II) perchlorate hydrate [ No CAS ]
  • Fe(2,6-bis(pyrazol-3-yl)pyridine)2(ClO4)2 [ No CAS ]
  • 31
  • [ 63285-53-0 ]
  • iron(II) perchlorate hexahydrate [ No CAS ]
  • [ 64-17-5 ]
  • [ 620945-45-1 ]
  • Fe(2,6-bis(pyrazol-3-yl)pyridine)2[Cr(bpy)(Ox)2]ClO4*EtOH*4H2O [ No CAS ]
  • 32
  • [ 63285-53-0 ]
  • iron(II) perchlorate hexahydrate [ No CAS ]
  • [ 64-17-5 ]
  • [ 371253-41-7 ]
  • Fe(2,6-bis(pyrazol-3-yl)pyridine)2[Cr(phen)(Ox)2]ClO4*1.5EtOH*4H2O [ No CAS ]
  • 33
  • [ 109-65-9 ]
  • [ 63285-53-0 ]
  • [ 1240464-19-0 ]
  • 34
  • [ 693-67-4 ]
  • [ 63285-53-0 ]
  • [ 1240464-22-5 ]
  • 35
  • [ 63285-53-0 ]
  • [ 111-25-1 ]
  • [ 1240464-20-3 ]
  • 36
  • [ 63285-53-0 ]
  • [ 112-29-8 ]
  • [ 1240464-21-4 ]
  • 37
  • [ 63285-53-0 ]
  • [ 112-71-0 ]
  • [ 1240464-24-7 ]
  • 38
  • [ 63285-53-0 ]
  • [ 544-77-4 ]
  • [ 1240464-25-8 ]
  • 39
  • [ 63285-53-0 ]
  • [ 143-15-7 ]
  • [ 1240464-23-6 ]
  • 40
  • [ 63285-53-0 ]
  • [ 112-89-0 ]
  • [ 1240464-26-9 ]
  • 41
  • [ 63285-53-0 ]
  • [ 74-88-4 ]
  • [ 1240464-27-0 ]
  • 42
  • [ 7357-67-7 ]
  • [ 63285-53-0 ]
  • [ 1240350-36-0 ]
  • 43
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • (iron(III))6(2,6-bis(pyrazol-3-yl)pyridine(-2H))4(μ3-O)2(μ-OMe)3(μ-OH)Cl2 [ No CAS ]
  • 44
  • [ 63285-53-0 ]
  • [ 1315594-60-5 ]
  • [ 1315594-59-2 ]
  • 45
  • [ 63285-53-0 ]
  • [ 106-95-6 ]
  • [ 1332491-99-2 ]
  • 46
  • [ 1129-30-2 ]
  • [ 4637-24-5 ]
  • [ 63285-53-0 ]
  • 47
  • [ 63285-53-0 ]
  • cadmium(II) nitrate tetrhydrate [ No CAS ]
  • 4-(trimethylammonio)benzene thiolate hexafluorophosphate [ No CAS ]
  • [Cd(4-(trimethylammonio)benzenethiolate(1-))2(2,6-bis(pyraz-3-yl)pyridine)](PF6)2 [ No CAS ]
  • 48
  • [ 63285-53-0 ]
  • dysprosium(III) nitrate hydrate [ No CAS ]
  • [ 67-68-5 ]
  • [Dy4(2,6-di(pyrazole-3-yl)pyridine)3(CO3)6(H2O)3]*DMSO*18H2O [ No CAS ]
  • 49
  • [ 63285-53-0 ]
  • copper(II) choride dihydrate [ No CAS ]
  • [ 446035-99-0 ]
  • 50
  • [ 63285-53-0 ]
  • [ 10025-76-0 ]
  • [Eu(2,6-bis(1H-pyrazol-3-yl)pyridine)Cl(H2O)5]Cl2 [ No CAS ]
  • 51
  • [ 63285-53-0 ]
  • [ 10025-76-0 ]
  • [Eu(2,6-bis(1H-pyrazol-3-yl)pyridine)2Cl(H2O)2]Cl2 [ No CAS ]
  • 52
  • [ 63285-53-0 ]
  • manganese(II) perchlorate tetrahydrate [ No CAS ]
  • [ 4923-84-6 ]
  • [Mn3(t-BuPO3)2(2,6-bis(pyrazol-3-yl)pyridine)3](ClO4)2*H2O [ No CAS ]
  • 53
  • [ 63285-53-0 ]
  • [ 13755-29-8 ]
  • iron(II) chloride [ No CAS ]
  • [ 111994-63-9 ]
  • 54
  • [ 63285-53-0 ]
  • [ 13755-29-8 ]
  • manganese(ll) chloride [ No CAS ]
  • iron(II) chloride [ No CAS ]
  • Fe0.85Mn0.15(2,6-bis(pyrazol-3-yl)pyridine)2(BF4)2 [ No CAS ]
  • 55
  • [ 63285-53-0 ]
  • [ 13755-29-8 ]
  • manganese(ll) chloride [ No CAS ]
  • iron(II) chloride [ No CAS ]
  • [(iron(II))0.948(manganese(II))0.052(2,6-bis(pyrazol-3-yl)pyridine)2](BF4)2 [ No CAS ]
  • 56
  • [ 63285-53-0 ]
  • [ 13755-29-8 ]
  • manganese(ll) chloride [ No CAS ]
  • iron(II) chloride [ No CAS ]
  • [(iron(II))0.902(manganese(II))0.098(2,6-bis(pyrazol-3-yl)pyridine)2](BF4)2 [ No CAS ]
  • 57
  • [ 63285-53-0 ]
  • [ 13755-29-8 ]
  • manganese(ll) chloride [ No CAS ]
  • Mn(2,6-bis(pyrazol-3-yl)pyridine)2(BF4)2 [ No CAS ]
  • 58
  • [ 63285-53-0 ]
  • iron(II) perchlorate monohydrate [ No CAS ]
  • [ 60-29-7 ]
  • [ 67-64-1 ]
  • C22H18FeN10(2+)*2ClO4(1-)*1.75C3H6O*1.5C4H10O [ No CAS ]
  • 59
  • [ 63285-53-0 ]
  • [ 52462-29-0 ]
  • [ 25108-36-5 ]
  • [ 1402044-84-1 ]
  • 60
  • [ 63285-53-0 ]
  • [ 52462-29-0 ]
  • 2-quinolinecarboxylic acid potassium salt [ No CAS ]
  • [ 1402044-85-2 ]
  • 61
  • [ 63285-53-0 ]
  • [ 1220653-10-0 ]
  • [ 1402044-84-1 ]
  • 62
  • [ 63285-53-0 ]
  • [ 1402044-79-4 ]
  • [ 1402044-85-2 ]
  • 63
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • potassium dicyanoargentate(I) [ No CAS ]
  • [Fe(2,6-bis[1H-pyrazol-3-yl]pyridine)2][Ag(CN)2]2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
64% In water; General procedure: A mixture of FeCl2·4H2O (0.12g, 0.59mmol) and 3-bpp (0.25g, 1.18mmol) in water (50cm3) was stirred with mild heating until all the solid had dissolved. The resultant orange-brown solution was filtered, and an aqueous solution of K[Ag(CN)2] (0.23g, 1.18mmol in 10cm3 H2O) was slowly added to the filtrate giving an immediate orange precipitate. The precipitate was allowed to settle overnight, then collected by filtration, washed with water and dried in vacuo. The solid product is sparingly soluble in most organic solvents, but can be recrystallised in mg quantities from 2,2,2-trifluoroethanol/ diethyl ether to yield plate-like crystals of the monohydrate material. Yield 0.20g, 64%. Anal. Calc. for C26H18Ag2FeN14: C, 39.1; H, 2.27; N, 24.6. Found: C, 39.2; H, 2.20; N, 24.0%. ES mass spectrum (MeCN) m/z 212.1 [3-bpp+H]+, 234.1 [Na(3-bpp)]+, 318.0 [Ag(3-bpp)]+, 445.2 [Na(3-bpp)2]+, 529.1 [Ag(3-bpp)2]+, 637.0 [Fe(3-bpp)2Ag(CN)2]+. IR (nujol): 3144s, 3096m, 2149s, 1615m, 1573m, 1562m, 1540w, 1532m, 1515m, 1435s, 1353m, 1304w, 1281m, 1230w, 1165w, 1148m, 1105w, 1083w, 1068m, 1025w, 996m, 929m, 883m, 841m, 764s, 615m cm-1.
  • 64
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • potassium dicyanoaurate [ No CAS ]
  • [Fe(2,6-bis[1H-pyrazol-3-yl]pyridine)2][Au(CN)2]2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
64% In water; v
  • 65
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • potassium bis(thiocyanato)aurate(I) [ No CAS ]
  • [Fe(2,6-bis[1H-pyrazol-3-yl]pyridine)2][Au(SCN)2]2*2,2,2-trifluoroethanol [ No CAS ]
YieldReaction ConditionsOperation in experiment
64% In water; Method as for 1, using K[Au(SCN)2] (0.42g, 1.18mol). The product was an orange powder, that formed polycrystalline needles from 2,2,2-trifluoroethanol/ diethyl ether. Yield 0.20g, 64%. Anal. Calc. for C26H18Au2FeN14S4·CF3CH2OH: C, 27.9; H, 1.84; N, 16.3. Found C, 27.0; H, 1.90; N, 15.9%. ES mass spectrum (MeCN) m/z 212.1 [LH]+, 445.2 [Na(3-bpp)2]+, 477.1 [Fe(3-bpp)2]+, 523.2 ([Au(3-bpp-H)(SCN)2]+), 581.1 ([Fe(3-bpp)Au(SCN)2]+), 735.2 ([Au(3-bpp)2(SCN)2]+), 792.2 ([Fe(3-bpp)2Au(SCN)2]+). IR (nujol): 3161s, 3134s, 2131s, 1614m, 1573s, 1514m, 1435s, 1353s, 1305m, 1282m, 1233m, 1169m, 1149s, 1104w, 1084m, 1065s, 1019w, 994s, 960w, 927m, 877s, 810s, 767s, 738m, 692w, 667m, 614s cm-1.
  • 66
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • [ 143-66-8 ]
  • [Fe(2,6-bis[1H-pyrazol-3-yl]pyridine)2][B(Ph)4]2*1/2H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
89% In water; A mixture of FeCl2·4H2O (0.12g, 0.59mmol) and 3-bpp (0.25g, 1.18mmol) in water (50cm3) was stirred with mild heating until all the solid had dissolved. The resultant orange-brown solution was filtered, and an aqueous solution of NaBPh4 (0.40g, 1.18mmol in 20cm3 H2O) was slowly added to the filtrate giving an immediate yellow precipitate. The solid was collected by filtration, washed with water and dried in vacuo. Recrystallisation from MeNO2/Et2O yielded yellow plates, which decomposed in vacuo to an orange-brown powder. Yield 0.59g, 89%. Anal. Calc. for C70H58B2FeN10·H2O: C, 75.7; H, 5.28; N, 12.4. Found: C, 74.9; H, 5.15; N, 12.6%. ES mass spectrum (MeCN) m/z 212.1 [3-bpp+H]+, 234.1 [Na(3-bpp)]+, 477.1 [Fe(3-bpp)2]+. IR (nujol) 3584w, 3513w, 3387s, 3346s, 3143m, 3119m, 3054w, 3031w, 1950br w, 1884br w, 1826br w, 1647br w, 1609m, 1579m, 1507w, 1497w, 1531w, 1359s, 1303w, 1274m, 1216m, 1090m, 1065m, 1032m, 991m, 971w, 960w, 931m, 916w, 864w, 845m, 812m, 775s, 744s, 737s, 709s, 670w, 642w, 628w, 610m cm-1.
  • 67
  • [ 63285-53-0 ]
  • [ 100-39-0 ]
  • [ 1464008-49-8 ]
YieldReaction ConditionsOperation in experiment
45% With lithium hydride; In tetrahydrofuran; for 44.0h;Reflux; Inert atmosphere; 2,6-Bis(pyrazol-3-yl)pyridine (2.00 g, 9.5 mmol) and lithium hydride (0.22 g, 28.4 mmol) were suspended in dry THF, in the presence of benzyl bromide (4.86 g, 28.4 mmol). The mixture was then heated at reflux for 44 h under a nitrogen atmosphere. The resultant white precipitate was removed via filtration and washed with water. The solid was then recrystallised from chloroform and dried in vacuo. Yield 1.67 g, 45%.
  • 68
  • [ 75-30-9 ]
  • [ 63285-53-0 ]
  • [ 1464008-51-2 ]
YieldReaction ConditionsOperation in experiment
95% With lithium hydride; In tetrahydrofuran; for 72.0h;Reflux; Inert atmosphere; The same method as described for LBz was followed, using 2-iodopropane (4.83 g, 28.4 mmol). After 72 h at reux under a nitrogen atmosphere, the resultant white precipitate was collected, washed with water and dried in vacuo. The product was employed without further purication. Yield 2.67 g, 95%.
  • 69
  • [ 63285-53-0 ]
  • iron(II) perchlorate hexahydrate [ No CAS ]
  • [ 1574222-35-7 ]
  • [ 67-64-1 ]
  • [Fe(2,6-bis(pyrazol-3-yl)pyridine)(2,6-bis(5-(2-methoxyphenyl)pyrazol-3-yl)pyridine)](perchlorate)2*1.5C3H6O [ No CAS ]
  • 70
  • [ 63285-53-0 ]
  • iron(III) chloride [ No CAS ]
  • [ 1610525-25-1 ]
  • 71
  • [ 63285-53-0 ]
  • iron(II) tetrafluoroborate hexahydrate [ No CAS ]
  • [ 7732-18-5 ]
  • [(4-dimethylamino-2,6-bis(1,1-bis(2-pyridyl)ethyl)pyridine)Fe(H2O)](BF4)2*H2O [ No CAS ]
  • 72
  • [ 67-56-1 ]
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • [ 46190-30-1 ]
  • [ 7732-18-5 ]
  • [Fe(bpp)2](C8H4O4)·2CH3OH·H2O [ No CAS ]
  • [Fe(bpp)2](C8H4O4)·5H2O [ No CAS ]
  • 73
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • 0.1C6H10O4*Ba(2+)*C6H8O4(2-) [ No CAS ]
  • [ 7732-18-5 ]
  • [Fe(bpp)2](C6H8O4)·4H2O [ No CAS ]
  • 74
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • C22H18FeN10(2+)*2Cl(1-)*2H2O [ No CAS ]
  • 75
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • [Fe(2,6-bis-(pyrazol-3-yl)pyridine)2]Cl2 [ No CAS ]
  • 76
  • [ 67-56-1 ]
  • [ 63285-53-0 ]
  • iron(II) chloride tetrahydrate [ No CAS ]
  • 6Fe(3+)*4C11H7N5(2-)*2O(2-)*3.67CH3O(1-)*0.33HO(1-)*2Cl(1-)*0.33CH4O*H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
41% With silver(I) nitrite; for 1.0h;Inert atmosphere; Schlenk technique; A 50-mL Schlenk flask was charged with 50 mg (0.25 mmol) of FeCl2∘4H2O and 210 mg (1.00 mmol) of 3-H2bpp, and 20 mL ofmethanol was added with stirring to result in a clear gold-yellowsolution. To this solution was added 230 mg (1.50 mmol) of AgNO2,and the reaction mixture was stirred for 1 h. After this time, a black precipitate that formed was filtered off via cannula. The dark orange solution obtained was allowed to slowly evaporate under a flow of N2 gas or layered with anhydrous diethyl ether. In both cases, X-ray quality single crystals were obtained within a few days. The crystals were isolated by filtration, washed with cold MeOH, and dried under suction. Yield = 24 mg (41%). Anal. Calc. (Found) for Fe6Cl2O7.66N20C48H43.3 (1),%: C 41.3 (40.35), H 3.22(3.06), N 18.8 (19.61).
  • 77
  • [ 63285-53-0 ]
  • iron(II) sulfate hexahydrate [ No CAS ]
  • potassium dicyanoaurate [ No CAS ]
  • [Fe(2,6-di-(1H-pyrazol-3-yl)pyridine)2][Au(CN)2]2 [ No CAS ]
  • 78
  • [ 67-56-1 ]
  • [ 63285-53-0 ]
  • iron(III) chloride [ No CAS ]
  • C11H9Cl3FeN5 [ No CAS ]
YieldReaction ConditionsOperation in experiment
89% for 0.5h; Anhydrous ferric chloride (0.041 g, 0.25 mmol) was added to a solution of 2,6-bis(1-hydro-3-pyrazole)pyridine (0.053 g, 0.25 mmol) in methanol (20 mL). The solution was stirred for 0.5 h, filtered, and the filtrate was diluted with diethyl ether. After two days, a large amount of red crystals were obtained, filtered, washed with diethyl ether and dried in vacuo to give the desired product.[Fe(bppyH2)Cl3]·MeOH, weighed.Yield: 0.084 g, yield: 89%(calculated based on ligand bppyH2)
  • 79
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • 2C6H4NO3(1-)*Ba(2+)*4H2O [ No CAS ]
  • C22H18FeN10(2+)*2C6H4NO3(1-)*2.4H2O [ No CAS ]
  • 80
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • 2C6H4NO3(1-)*Ba(2+)*4H2O [ No CAS ]
  • C22H18FeN10(2+)*2C6H4NO3(1-)*1.8H2O*0.6(2)H2O [ No CAS ]
  • 81
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • 0.1C6H10O4*Ba(2+)*C6H8O4(2-) [ No CAS ]
  • C22H18FeN10(2+)*C6H8O4(2-)*4H2O [ No CAS ]
  • 82
  • [ 63285-53-0 ]
  • ferrous(II) sulfate heptahydrate [ No CAS ]
  • [ 2923-18-4 ]
  • [Fe(2,6-bis(pyrazol-3-yl)pyridine)2](CF3COO)2 [ No CAS ]
  • 83
  • [ 331942-32-6 ]
  • [ 63285-53-0 ]
YieldReaction ConditionsOperation in experiment
75 % With hydrazine hydrate In ethanol at 120℃; Green chemistry; 3.3. General Procedure for Preparation of Bis(azoles) 4 and 5 General procedure: Method I: For bis(pyrazoles), A mixture of compound 3 (10 mmol) and hydrazinemonohydrate (20 mmol) in ethanol was refluxed at 50-60 C for 120 min. The mixture wasleft to cool and then added to iced water. The solid was collected by filtration and washedby EtOH. For bis(isoxazoles), a mixture of compound 3 (10 mmol), hydroxylamine hydrochloride(25 mmol) and sodium carbonate (25 mmol) in EtOH was refluxed at 50-60 Cfor 240 min. The mixture was left to cool and then added to iced water. The solid wascollected by filtration and washed by EtOH.
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