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[ CAS No. 63352-97-6 ] {[proInfo.proName]}

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Product Details of [ 63352-97-6 ]

CAS No. :63352-97-6 MDL No. :MFCD09965681
Formula : C10H8BrNO2 Boiling Point : -
Linear Structure Formula :- InChI Key :XYQBUBGQOKPXBN-UHFFFAOYSA-N
M.W : 254.08 Pubchem ID :12344554
Synonyms :

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Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 63352-97-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 63352-97-6 ]

[ 63352-97-6 ] Synthesis Path-Downstream   1~2

YieldReaction ConditionsOperation in experiment
85% Stage #1: With morpholine; sulfur at 120℃; for 6h; Stage #2: With sodium hydroxide In ethanol for 4h; Reflux; General procedure: It will be apparent to those skilled in the art that various modifications that may be derived or recited directly from the disclosure and common sense of the present patent, as well as by the prior art, are well known in the art, Such as changing the substituents on the indole ring or changing the position of the substituents, the solvent of the reaction solvent not indicated in the specification, the change in the reaction temperature, the time, the change of the acid and the base, and the like Non-substantive changes, the same can be applied, can achieve the patent description of the function and effect, no longer one by one for example, are within the scope of this patent
3-Formylpropionsaeure, 2-Bromphenylhydrazin;
YieldReaction ConditionsOperation in experiment
24% 5.a Example 5(a) Example 5(a) 7-Bromoindole-3-acetic acid 7-bromoindole: Pale brown needles, yield 24%, m.p. 42-44°C (lit (Aldrich chemical catalogue) 41-44°C); m/z 197, 195 (M+).
24% 5.a 7-Bromoindole-3-acetic acid Example 5(a) 7-Bromoindole-3-acetic acid 7-bromoindole: Pale brown needles, yield 24%, m.p. 42-44° C. (lit (Aldrich chemical catalogue) 41-44° C.); m/z 197, 195 (M+).
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