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Chemical Structure| 635311-42-1 Chemical Structure| 635311-42-1

Structure of 635311-42-1

Chemical Structure| 635311-42-1

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Product Details of [ 635311-42-1 ]

CAS No. :635311-42-1
Formula : C13H15NO3
M.W : 233.26
SMILES Code : O=C(OCC1=CC=CC=C1)NC2CC(CC2)=O
MDL No. :MFCD16036402

Safety of [ 635311-42-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H319
Precautionary Statements:P264-P280-P305+P351+P338-P337+P313

Application In Synthesis of [ 635311-42-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 635311-42-1 ]

[ 635311-42-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 14150-94-8 ]
  • [ 635311-42-1 ]
  • [ 1119103-53-5 ]
  • [ 1119103-59-1 ]
YieldReaction ConditionsOperation in experiment
With ammonia; In methanol; at 90℃; for 0.5h;Microwave irradiation; A mixture of SP-0010418-2 (1.2 g, 5.128 mmol), 1-methyl-3,5-dinitropyridin- 2(1H)-one (1.53 g, 7.692 mmol) and 7.0 M NH3/MeOH (2.0 mL) in MeOH (8.0 mL) was stirred at 90 C for 0.5 h under microwave irridation. The residue was purified by silica gel column chromatography (using petroleum ether/EtOAc = 10:0 - 7:3) to give mixture SP0010418-162-3A and SP-0010418-162-3B (910 mg, yield: 57%). LC-MS 314 (M+H), 91%(UV2l4nm).
 

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