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Chemical Structure| 63659-30-3 Chemical Structure| 63659-30-3

Structure of 63659-30-3

Chemical Structure| 63659-30-3

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Product Details of [ 63659-30-3 ]

CAS No. :63659-30-3
Formula : C6H12O3S
M.W : 164.22
SMILES Code : CS(=O)(OCC1CCC1)=O
MDL No. :MFCD20482257

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Application In Synthesis of [ 63659-30-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 63659-30-3 ]

[ 63659-30-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 63659-30-3 ]
  • [ 61439-59-6 ]
  • [ 63659-31-4 ]
YieldReaction ConditionsOperation in experiment
80% In N-methyl-acetamide; Petroleum ether; 10 g of 2-(p-benzoxyphenyl)-ethanol are converted to the sodium derivative with 2.2 g of 50percent strength sodium hydride in dimethylformamide, with gentle heating to assist the reaction. 7.7 g (0.047 mol) of cyclobutylmethyl mesylate in 10 ml of the same solvent are then added. The reaction mixture is heated to 60°-70° for 18 hours and is poured into water and extracted with ether, and the extract is washed with water, dried over sodium sulphate and evaporated to dryness. The residual oil is taken up in petroleum ether, and insoluble material (2.3 g of the starting alcohol, which has not reacted) is filtered off, the solvent is evaporated and the residual oil is then distilled under reduced pressure. 8 g (yield=80percent) of 4-[2-(cyclobutylmethoxy)ethyl]-1-benzoxy-benzene are thus obtained.
 

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