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Chemical Structure| 6590-93-8 Chemical Structure| 6590-93-8

Structure of 6590-93-8

Chemical Structure| 6590-93-8

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Product Details of [ 6590-93-8 ]

CAS No. :6590-93-8
Formula : C7H3Cl2NS
M.W : 204.08
SMILES Code : ClC1=CC(Cl)=CC(N=C=S)=C1
MDL No. :MFCD00041072

Safety of [ 6590-93-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P280-P301+P330+P331-P302+P352-P304+P340-P305+P351+P338-P310
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 6590-93-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6590-93-8 ]

[ 6590-93-8 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 120-35-4 ]
  • [ 6590-93-8 ]
  • 3-[3-(3,5-dichlorophenyl)-thioureido]-4-methoxy-N-phenyl-benzamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethyl acetate; Example 60 3-[3-(3,5-Dichlorophenyl)-thioureido]-4-methoxy-N-phenyl-benzamide A mixture of 3-amino-4-methoxy-N-phenyl-benzamide (0.277 g, 1.14 mmol) and 3,5-dichlorophenyl isothiocyanate (0.238 g, 1.17 mmol) in ethyl acetate (30 mL) was warmed until a solution was obtained, then allowed to stand at room temperature for 3 days. The reaction was concentrated until a crystalline precipitate was obtained then allowed to stand overnight at room temperature. The solid was collected by filtration, rinsed with ethyl acetate/hexane, and dried to afford the product (0.423 g); m.p. 195-197 C. Calculated for C21H17Cl2N3O2S: C, 56.51; H, 3.84; N, 9.41. Found: C, 56.20; H, 3.69; N, 9.28.
 

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