Alternatived Products of [ 65953-56-2 ]
Product Details of [ 65953-56-2 ]
CAS No. : | 65953-56-2 |
MDL No. : | MFCD09264744 |
Formula : |
C16H30N4O2S
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
342.50
|
Pubchem ID : | - |
Synonyms : |
|
Safety of [ 65953-56-2 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 65953-56-2 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 65953-56-2 ]
- 1
-
[ 65915-94-8 ]
-
[ 65953-56-2 ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 2 steps
1: 88 percent / N-methylmorpholine; HATU / dimethylformamide / 20 °C
2: 90 percent / HCl / ethyl acetate / 0.5 h |
|
Reference:
[1]Sabatino, Giuseppina; Chinol, Marco; Paganelli, Giovanni; Papi, Stefano; Chelli, Mario; Leone, Giuseppe; Papini, Anna Maria; De Luca, Angelo; Ginanneschi, Mauro
[Journal of Medicinal Chemistry, 2003, vol. 46, # 14, p. 3170 - 3173]
- 2
-
[ 124-09-4 ]
-
[ 33755-53-2 ]
-
[ 65953-56-2 ]
Yield | Reaction Conditions | Operation in experiment |
90% |
With pyridine In water at 20℃; for 24h; |
|
Reference:
[1]Location in patent: experimental part
Lu, Liang; Gu, Xiaorong; Hong, Li; Laird, James; Jaffe, Keeve; Choi, Jaewoo; Crabb, John; Salomon, Robert G.
[Bioorganic and Medicinal Chemistry, 2009, vol. 17, # 21, p. 7548 - 7561]
- 3
-
[ 175281-76-2 ]
-
[ 65953-56-2 ]
-
N-biotinamido-N'-(α-methyl nitroveratryl)butyryl-1,6-diaminohexane
[ No CAS ]
- 4
-
[ 103946-54-9 ]
-
[ 65953-56-2 ]
-
C28H38N6O3S
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
69.4% |
|
A mixture of 0.44 g (2.05 mmol) of 4-methyl-2,2-bipyridine-4-carboxylic acid,0.39 g EDC (2.05 mmol) and 0.24 g NHS (2.55 mmol) were dissolved in DMF,Heated to 60 C for 2 h,Further, 0.70 g of product 4 (2.05 mmol) obtained in step (1) and 1 mL of triethylamine were added for 24 h,Followed by addition of ice water, suction filtration to give product 7, yield 69.4% |