Home Cart Sign in  
Chemical Structure| 66790-60-1 Chemical Structure| 66790-60-1

Structure of 66790-60-1

Chemical Structure| 66790-60-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

DE Stock

US Stock

Asia Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 66790-60-1 ]

CAS No. :66790-60-1
Formula : C10H11BrO2
M.W : 243.10
SMILES Code : O=C(O)CCC1=CC=CC(C)=C1Br
MDL No. :MFCD18392245

Safety of [ 66790-60-1 ]

Application In Synthesis of [ 66790-60-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 66790-60-1 ]

[ 66790-60-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2033-24-1 ]
  • [ 109179-31-9 ]
  • [ 66790-60-1 ]
YieldReaction ConditionsOperation in experiment
3.9 g With formic acid; triethylamine; at 100℃; for 2h; Step 1 (0503) A mixture of <strong>[109179-31-9]2-bromo-3-methylbenzaldehyde</strong> (3.15 g), 2,2-dimethyl-[1,3]dioxane-4,6-dione (2.28 g), triethylamine (3 mL) and formic acid (2 mL) was stirred at an external temperature of 100° C. for 2 hours. The mixture was cooled to room temperature. The mixture was poured into ice water, and the resulting mixture was diluted with hydrochloric acid (2 mol/L) and ethyl acetate. The ethyl acetate layer was washed with brine, and concentrated under reduced pressure to give 3-(2-bromo-3-methylphenyl)propionic acid (3. 90 g).
 

Historical Records

Technical Information

Categories