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Chemical Structure| 67159-81-3 Chemical Structure| 67159-81-3

Structure of 67159-81-3

Chemical Structure| 67159-81-3

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Product Details of [ 67159-81-3 ]

CAS No. :67159-81-3
Formula : C11H13NO
M.W : 175.23
SMILES Code : O=C1CC(C)(C)C2=C1C=C(N)C=C2

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Application In Synthesis of [ 67159-81-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 67159-81-3 ]

[ 67159-81-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67159-81-3 ]
  • [ 7205-46-1 ]
  • [ 1449515-47-2 ]
YieldReaction ConditionsOperation in experiment
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; for 15h;Reflux; To a solution of 6-chloro-l -methyl- lH-imidazo[4,5-c]pyridine (intermediate 2) (14.9 mmol) in dioxane (100 mL) is added the corresponding aniline (22.4 mmol), cesium carbonate (22.4 mmol), BINAP (0.9mmol) and tris(dibenzylideneacetone)dipalladium (0.45 mmol). The reaction mixture is refluxed for 15 h, filtrated on celite, evaporated to dryness and purified on silica gel to give the expected product.
 

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