Home Cart Sign in  
Chemical Structure| 6746-22-1 Chemical Structure| 6746-22-1

Structure of 6746-22-1

Chemical Structure| 6746-22-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 6746-22-1 ]

CAS No. :6746-22-1
Formula : C28H28Sn
M.W : 483.23
SMILES Code : CC1=CC=C([Sn](C2=CC=C(C)C=C2)(C3=CC=C(C)C=C3)C4=CC=C(C)C=C4)C=C1
MDL No. :MFCD00048088

Safety of [ 6746-22-1 ]

Application In Synthesis of [ 6746-22-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6746-22-1 ]

[ 6746-22-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 120-72-9 ]
  • [ 6746-22-1 ]
  • [ 55577-25-8 ]
YieldReaction ConditionsOperation in experiment
70% With [Pd(OTs)2(MeCN)2]; oxygen; acetic acid; at 25℃; for 12h;Schlenk technique; General procedure: In a Schlenk tube equipped with a magnetic stir bar, indole 1 (or 4 or 6) (0.5 mmol, 1.0 equive), tetraarylstannane 2 (0.19 mmol), and (MeCN)2Pd(OTs)2(0.05 mmol) were added. HOAc (5 mL) was introduced by a syringe. The reaction tube was degassed (3 times), charged with dioxygen gas and kept under an oxygen atmosphere by using an oxygen balloon. After stirring at 25 C for the time indicated, HOAc was removed via rotary evaporation, and the residue was dissolved in DCM (50mL) and washed with aqueous NaHCO3 (2 × 30 mL). The organic layers were combined, washed with brine, and dried over anhydrous Na2SO4. The solvent was removed via rotary evaporation and the crude product was purified by column chromatography on silica gel using DCM/petroleum ether to afford the desired product.
 

Historical Records