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Chemical Structure| 676578-20-4 Chemical Structure| 676578-20-4

Structure of 676578-20-4

Chemical Structure| 676578-20-4

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Product Details of [ 676578-20-4 ]

CAS No. :676578-20-4
Formula : C20H21BO2
M.W : 304.19
SMILES Code : CC1(C)C(C)(C)OB(C2=CC=C3C=C4C=CC=CC4=CC3=C2)O1
MDL No. :MFCD30471374
InChI Key :PHGAEOZJPSSSIV-UHFFFAOYSA-N
Pubchem ID :59464627

Safety of [ 676578-20-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 676578-20-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 676578-20-4 ]

[ 676578-20-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 870119-58-7 ]
  • [ 676578-20-4 ]
  • [ 302571-01-3 ]
  • 6-(3-(9H-carbazole-9-yl)phenyl)-2-(anthracene-2-yl)-9H-carbazole [ No CAS ]
YieldReaction ConditionsOperation in experiment
1) In a 500ml three-neck bottle,Add 3,7-dibromo-9H-carbazole (32.50 g, 100 mmol),3-(9H-carbazol-9-yl)benzene borate (36.93 g, 100 mmol),Potassium carbonate (27.64 g, 200 mmol), 150 g of toluene, 75 g of ethanol,75g water, tetrakis(triphenylphosphine)palladium was added under the protection of N2, and reacted at 85 C for 12 h.The TLC monitors the completion of the reaction and begins to cool down. After falling to room temperature,Add thiol-2-borate (30.42 g, 100 mmol) to a three-necked flask.The reaction was carried out at 85 C for 12 h, and the reaction was completed by TLC. After cooling to room temperature,The reaction solution was washed twice with water (200 ml), and the mixture was separated to give an organic phase.Filtration, distilling off the solvent under reduced pressure, and then recrystallizing twice with ethyl acetate.Drying under vacuum gave the intermediate 6-(3-(9H-carbazol-9-yl)phenyl)-2-(indol-2-yl)-9H-indazole.
  • 2
  • [ 870119-58-7 ]
  • [ 676578-20-4 ]
  • [ 302571-01-3 ]
  • C68H40N4S [ No CAS ]
 

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