Home Cart Sign in  
Chemical Structure| 68305-76-0 Chemical Structure| 68305-76-0

Structure of 68305-76-0

Chemical Structure| 68305-76-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 68305-76-0 ]

CAS No. :68305-76-0
Formula : C12H17NO4S
M.W : 271.33
SMILES Code : CC(C)C[C@@H](C(O)=O)NS(=O)(C1=CC=CC=C1)=O
MDL No. :MFCD09749741

Safety of [ 68305-76-0 ]

Application In Synthesis of [ 68305-76-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 68305-76-0 ]

[ 68305-76-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 68305-76-0 ]
  • [ 192725-45-4 ]
  • C40H47F3N4O5S [ No CAS ]
YieldReaction ConditionsOperation in experiment
Same as Example 2, except that the amine group and amido group of compound 22 were deprotected to obtain compound 3.15 mg of compound 22 in Example 2 was treated with 9:1 trifluoroacetic acid (TFA): CH2Cl2 for 30 minutes, and the solvent was removed by co-evaporation with toluene. Under the protection of nitrogen, the residue obtained was mixed with N-benzenesulfonylvaline. The mixed solution of tetramethylurea tetrafluoroborate, triethylamine and dimethylformamide was reacted at room temperature for 10 hours to obtain compound 3, which was confirmed by LCMS detection to have the stated structure.
  • 2
  • [ 68305-76-0 ]
  • [ 192725-45-4 ]
  • C40H49N3O5S [ No CAS ]
YieldReaction ConditionsOperation in experiment
(9) Add compound 17 and an equimolar amount of 2,6-dimethylphenol acetic acid to tetramethylurea tetrafluoroborate (TBTU), triethylamine (Et3N) and dimethylformamide (DMF) Stir at room temperature for 10 hours to obtain compound 22 respectively. Compound 22 was subjected to acidic conditions to remove the Boc group, 15 mg of compound 22 was dissolved in 9:1 trifluoroacetic acid: H2O, stirred at room temperature for 30 minutes, and toluene was added After evaporation to dryness, the obtained residue was coupled with N-benzenesulfonylvaline in a mixed solvent of tetramethylurea tetrafluoroborate, triethylamine and dimethylformamide to obtain compound 5, which was confirmed by LCMS The resulting compound 5 is the structure.
 

Historical Records